2,4-二甲氧基-1-氟苯合成路线 （共 18 条）
反应条件
1-(chloromethyl)-4-fluoro-1,4-diazoniabicyclo-[2.2.2]octane bis(tetrafluoroborate) in water; acetonitrile T=50°C; 0.5 h;
参考文献
Bacci, James P.; Kearney, Aaron M.; Van Vranken, David L.
Journal of Organic Chemistry, 2005 , vol. 70, # 22 p. 9051 - 9053
反应条件
1-chloromethyl-4-fluoro-1,4-diazoniabicyclo[2.2.2]octan*2BF4 T=85 - 90°C;
参考文献
Tetrahedron Letters, , vol. 48, # 15 p. 2671 - 2673
反应条件
AcOF in dichloromethane; monofluoro-trichloromethane T=-75°C;
参考文献
Journal of Organic Chemistry, , vol. 49, p. 806 - 813
反应条件
CsSO4F in acetonitrile 1 h; Ambient temperature;
参考文献
Stavber, Stojan; Kosir, Iztok; Zupan, Marko
Journal of the Chemical Society, Chemical Communications, 1992 , # 3 p. 274 - 275
反应条件
1: 96 percent / methanol / Heating 2: 100 percent / H2 / Pd/C / ethanol; ethyl acetate / 2068.6 Torr 3: 1.) NaNO2, HCl, 2.) H3PO2 / 1.) H2O, 15 min, 2.) H2O, 4 deg C, overnight, 20 deg C, 2 h View Scheme
参考文献
Journal of Organic Chemistry, , vol. 62, # 19 p. 6469 - 6475
反应条件
1: 100 percent / H2 / Pd/C / ethanol; ethyl acetate / 2068.6 Torr 2: 1.) NaNO2, HCl, 2.) H3PO2 / 1.) H2O, 15 min, 2.) H2O, 4 deg C, overnight, 20 deg C, 2 h View Scheme
参考文献
Journal of Organic Chemistry, , vol. 62, # 19 p. 6469 - 6475
反应条件
hydrogenchloride; hypophosphorous acid; sodium nitrite 1.) H2O, 15 min, 2.) H2O, 4 deg C, overnight, 20 deg C, 2 h; Yield given. Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 62, # 19 p. 6469 - 6475
参考文献
Davis, Franklin A.; Han, Wei
Tetrahedron Letters, 1991 , vol. 32, # 13 p. 1631 - 1634
反应条件
CsSO4F in acetonitrile
参考文献
Journal of Fluorine Chemistry, , vol. 54, # 1-3 p. 268
反应条件
CsSO4F in acetonitrile
参考文献
Journal of Fluorine Chemistry, , vol. 54, # 1-3 p. 268
