2,4-二甲氧基-1-氟苯合成路线 （共 18 条）
反应条件
1: 79 percent / fluoroboric acid, sodium nitrite / H2O 2: 59 percent / heating, distillation View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1658 - 1666
反应条件
1-(chloromethyl)-4-fluoro-1,4-diazoniabicyclo-[2.2.2]octane bis(tetrafluoroborate) T=70°C; 3 h; Ionic liquid;
参考文献
Molecules, , vol. 14, # 7 p. 2394 - 2409
反应条件
heating, distillation; Title compound not separated from byproducts;
参考文献
Durrani, Aziz A.; Tyman, John H. P.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1658 - 1666
反应条件
boron tribromide in dichloromethane
参考文献
Sun, Wei-Chuan; Gee, Kyle R.; Klaubert, Dieter H.; Haugland, Richard P.
Journal of Organic Chemistry, 1997 , vol. 62, # 19 p. 6469 - 6475
反应条件
boron tribromide in dichloromethane -78 deg C, RT, 30 min;
参考文献
Belanger, Patrice C.; Lau, C. K.; Williams, Haydn W. R.; Dufresne, C.; Scheigetz, John
Canadian Journal of Chemistry, 1988 , vol. 66, p. 1479 - 1482
反应条件
boron tribromide in dichloromethane -78 deg C, RT, 30 min;
参考文献
Belanger, Patrice C.; Lau, C. K.; Williams, Haydn W. R.; Dufresne, C.; Scheigetz, John
Canadian Journal of Chemistry, 1988 , vol. 66, p. 1479 - 1482
反应条件
boron tribromide in dichloromethane -78 deg C, RT, 30 min;
参考文献
Belanger, Patrice C.; Lau, C. K.; Williams, Haydn W. R.; Dufresne, C.; Scheigetz, John
Canadian Journal of Chemistry, 1988 , vol. 66, p. 1479 - 1482
反应条件
1: AlCl3 / CH2Cl2 / 68 h / 0 - 20 °C
2: 3.3 g / aq. HCl / 0 °C
View Scheme
参考文献
Chen, Chien-An; Yeh, Ren-Hwa; Lawrence, David S.
Journal of the American Chemical Society, 2002 , vol. 124, # 15 p. 3840 - 3841
