反应条件
1: 1.) AgNO3, pyridine, 2.) pyridine, H2S / 1.) MeOH, CH3CN, 0 deg C, 30 min, 2.) CH2Cl2, 0 deg C, 30 min; room temperature, 1 h
2: 15.8 g / DMAP, DCC / CH2Cl2 / 3 h / Ambient temperature
View Scheme
参考文献
Fuji, Masahiro; Watanabe, Fumihiko; Fujii, Yasuhiko; Hashizume, Hiroshi; Okuno, Takayuki; Shirahase, Kazuhiro; Teshirogi, Isao; Ohtani, Mitsuaki
Journal of Organic Chemistry, 1997 , vol. 62, # 20 p. 6804 - 6809
