3-(三甲基硅烷基)苯硼酸合成路线 （共 4 条）
反应条件
hydrogenchloride in water; pentane
参考文献
Burn, Paul Leslie; Samuel, Ifor David William; Cumpstey, Neil
Patent: US2008/211391 A1, 2008 ;
反应条件
1.1: BuLi / diethyl ether 1.2: diethyl ether 2.1: BuLi / diethyl ether 2.2: diethyl ether View Scheme
参考文献
Molecular Crystals and Liquid Crystals, , vol. 444, p. 95 - 101
反应条件
1: 1-bromo-3-trimethylsilanyl-benzene With n-butyllithium in diethyl ether 2: triethyl borane in diethyl ether
参考文献
Molecular Crystals and Liquid Crystals, , vol. 444, p. 95 - 101
反应条件
1: 40 percent / aq. NaOH / Pd(PPh3)4 / bis-(2-methoxy-ethyl) ether / 28 h / 60 - 80 °C
2: 86 percent / Br2 / CCl4 / 0.58 h / 0 °C
View Scheme
参考文献
King, Benjamin T.; Kroulik, Jiri; Robertson, Charles R.; Rempala, Pawel; Hilton, Cameron L.; Korinek, Justin D.; Gortari, Lisa M.
Journal of Organic Chemistry, 2007 , vol. 72, # 7 p. 2279 - 2288
