反应条件
1: NaNO3, HCl
2: 87 percent / Et3N / CH2Cl2; tetrahydrofuran / 1 h
3: 74 percent / LiAH4 / tetrahydrofuran / 0 deg C, 4 h, then -15 deg C, overnight
4: 42 percent / camphorsulfonic acid, 1,1,1-triacetoxy-1,1-dihydro-1,2-benziodoxol-3(1H)-one / 1 h / 0 °C
View Scheme
参考文献
Kelli-Basetti, Bernadette M.; Krodkiewska, Irena; Sasse, Wolfgang H. F.; Savage, G. Paul; Simpson, Gregory W.
Tetrahedron Letters, 1995 , vol. 36, # 2 p. 327 - 330
