乙基3-(三甲基硅基)丙酸酯合成路线 (共 12 条)
反应条件
potassium hydroxide in ethanol
参考文献
Nishitani, Kiyoshi; Yamakawa, Koji
Tetrahedron Letters, 1991 , vol. 32, # 3 p. 387 - 390
反应条件
1: 1.) n-BuLi, isopropylamine / 1) THF, 90 min, -78 deg C; 2) room temperature, 14 h 2: 92 percent / Et3N / diethyl ether / 1 h / 0 °C 3: 80 percent / diazabicyclo<5.4.0>undec-6-ene / diethyl ether / 12 h / Ambient temperature View Scheme
参考文献
Trost,B.M.; Chan,D.M.
Journal of the American Chemical Society, 1983 , vol. 105, p. 2326