反应条件
<b>Multi-step reaction with 6 steps<br /> </b>1: 71 percent / BuLi / tetrahydrofuran / 1.) 0 deg C, 30 min, 2.) -78 deg C, 2 h<br />2: 97 percent / HCl / 1 h / 20 °C<br />3: 93 percent / tetrahydrofuran / 3 h / 20 °C<br />4: 1.) MCPBA / 1.) CHCl<sub>3</sub>, 0 deg C, 30 min, 2.) r.t., 24 h<br />5: 86 percent / H<sub>2</sub> / 5percent Rh/Al<sub>2</sub>O<sub>3</sub> / ethanol / 20 h / 20 °C / 4560 Torr<br />6: 47 percent / POCl<sub>3</sub>, pyridine / 20 °C<br /> <br />
参考文献
Davies, Stephen G.; Smyth, G. Darren Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 20 p. 2467 - 2477
