2,3-二氢-2-重氮基-1H-茚-1-酮合成路线 （共 9 条）
反应条件
4-toluenesulfonyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene in dichloromethane T=30°C; 0.25 h;
参考文献
Rao, Y. Koteswar; Nagarajan, M.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1986 , vol. 25, p. 735 - 737
反应条件
1: With sodium methylate; formic acid ethyl ester in benzene T=20°C; Cooling with ice; 2: With 4-toluenesulfonyl azide; diethylamine in diethyl ether T=0 - 20°C;
参考文献
Vuluga, Daniela; Legros, Julien; Crousse, Benoit; Bonnet-Delpon, Daniele
Green Chemistry, 2009 , vol. 11, # 2 p. 156 - 159
参考文献
Dahn,H.; Ballenegger,M.
Helvetica Chimica Acta, 1969 , vol. 52, p. 2417 - 2427
参考文献
Cava et al.
Journal of the American Chemical Society, 1958 , vol. 80, p. 2257,2262
反应条件
in tetrahydrofuran; water
参考文献
Hooz,J. et al.
Canadian Journal of Chemistry, 1971 , vol. 49, p. 2371 - 2373
反应条件
perchloric acid in water T=25°C; Kinetics; Further Variations:SolventsReagents;
参考文献
Chiang, Yvonne; Kresge, A. Jerry; Sadovski, Oleg; Zeng, Xiaofeng; Zhu, Yu
Canadian Journal of Chemistry, 2005 , vol. 83, # 9 p. 1202 - 1206
参考文献
Tomioka, Hideo; Taketsuji, Kohji
Journal of Organic Chemistry, 1993 , vol. 58, # 16 p. 4196 - 4197
反应条件
methanol Irradiation.UV-Licht;
参考文献
Horner et al.
Chemische Berichte, 1958 , vol. 91, p. 430,436
反应条件
1: aqueous THF / Irradiation.UV-Licht
2: H2SO4; CHCl3; NaN3
View Scheme
参考文献
Horner et al.
Chemische Berichte, 1958 , vol. 91, p. 430,436
