2-氨基-5-硝基二苯甲酮合成路线 （共 35 条）
反应条件
in toluene 0.0333333 h; Microwave irradiation;
参考文献
Singh, Rajesh K.; Prasad; Bhardwaj
Medicinal Chemistry Research, 2013 , vol. 22, # 12 p. 5901 - 5911
反应条件
1.1: sulfuric acid; sodium nitrite / tetrahydrofuran; H2O / 15 h / 0 °C 1.2: 7 percent / potassium iodide / H2O / 1.5 h / Heating 2.1: 80 percent / H2; Et3N / 10percent Pd/C / methanol / 2.5 h / 20 °C / 760.05 Torr View Scheme
参考文献
Faucher, Nicolas; Ambroise, Yves; Cintrat, Jean-Christophe; Doris, Eric; Pillon, Florence; Rousseau, Bernard
Journal of Organic Chemistry, 2002 , vol. 67, # 3 p. 932 - 934
反应条件
sulfuric acid; acetic acid
Friedlaender condensation; 4 h; Reflux;
参考文献
Nedeltchev, Alexi K.; Han, Haesook; Bhowmik, Pradip K.
Tetrahedron, 2010 , vol. 66, # 48 p. 9319 - 9326
反应条件
1: With acetic acid; sodium nitrite in water
T=0°C; 1 h; Inert atmosphere;
2: With sodium azide in water
T=0 - 20°C; Inert atmosphere;
参考文献
Stokes, Benjamin J.; Vogel, Carl V.; Urnezis, Linda K.; Pan, Minjie; Driver, Tom G.
Organic Letters, 2010 , vol. 12, # 12 p. 2884 - 2887
反应条件
sodium acetate in (2S)-N-methyl-1-phenylpropan-2-amine hydrate; water; acetic acid; benzene
参考文献
Ciba-Geigy Corporation
Patent: US3943145 A1, 1976 ;
