1,4-二氢-1-甲基-3-吡啶甲酰胺合成路线 (共 7 条)
反应条件
1-benzyl-1,2-dihydroisonicotinamide in methanol 0.0833333 h; Ambient temperature;
参考文献
Nuvole, Antonio; Paglietti, Giuseppe; Sanna, Paolo; Acheson, R. Morrin
Journal of Chemical Research, Miniprint, 1984 , # 11 p. 3245 - 3256
反应条件
sodium dithionite; sodium carbonate in water
参考文献
Zielonka, Jacek; Marcinek, Andrzej; Adamus, Jan; Gebicki, Jerzy
Journal of Physical Chemistry A, 2003 , vol. 107, # 46 p. 9860 - 9864
反应条件
sodium dithionite; sodium hydrogencarbonate in chloroform; water T=4 - 5°C; 3 h; Title compound not separated from byproducts;
参考文献
Tetrahedron, , vol. 61, # 43 p. 10331 - 10337
反应条件
1: methanol / 20 °C 2: AgCl / H2O 3: 60 percent / aq. sodium dithionite; sodium carbonate / 0.33 h View Scheme
参考文献
Journal of Physical Chemistry A, , vol. 107, # 46 p. 9860 - 9864
参考文献
Srinivasan, R.; Medary, Richard T.; Fisher, Harvey F.; Norris, Donald J.; Stewart, Ross
Journal of the American Chemical Society, 1982 , vol. 104, # 3 p. 807 - 812
反应条件
in acetonitrile T=24.84°C; KineticsActivation energy;
参考文献
Zhu, Xiao-Qing; Deng, Fei-Huang; Yang, Jin-Dong; Li, Xiu-Tao; Chen, Qiang; Lei, Nan-Ping; Meng, Fan-Kun; Zhao, Xiao-Peng; Han, Su-Hui; Hao, Er-Jun; Mu, Yuan-Yuan
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 36 p. 6071 - 6089
反应条件
water; platinum
Hydrogenation;
参考文献
Karrer; Stare
Helvetica Chimica Acta, 1937 , vol. 20, p. 418,423