2-(二乙氨基乙基)-吡啶合成路线 (共 3 条)
反应条件
[Co(η5-C5H5)2] in tetrahydrofuran T=150°C; P=10640 Torr; 3 h;
参考文献
Ivanov, A. P.; Levin, D. Z.; Mortikov, E. S.; Promonenkov, V. K.
Journal of Organic Chemistry USSR (English Translation), 1989 , vol. 25, # 3.2 p. 566 - 570
Zhurnal Organicheskoi Khimii, 1989 , vol. 25, # 3 p. 629 - 633
反应条件
hydrogenchloride; sodium tetrahydroborate in methanol T=20°C; 72 h;
参考文献
Lin, Ya-Chi; Yu, Kuo-Hsuan; Lin, Ya-Fan; Lee, Gene-Hsiang; Wang, Yu; Liu, Shiuh-Tzung; Chen, Jwu-Ting
Dalton Transactions, 2012 , vol. 41, # 22 p. 6661 - 6670
反应条件
titanium; n-butyllithium; titanium tetrachloride 1.) hexane, room temp., 1 h; 2.) room temp., 15 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Betschart, Claudia; Seebach, Dieter
Helvetica Chimica Acta, 1987 , vol. 70, p. 2215 - 2231