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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
17759-15-8
合成路线
（共 9 条）
17759-15-8
→
反应条件
74502-83-3
2-(氯甲基)-4,6-二甲基嘧啶
反应条件
1: H2O / 20 h / 100 °C / sealed tube 2: 69 percent Spectr. / phosphoryl chloride / dioxane View Scheme
参考文献
Sakamoto, Takao; Yoshizawa, Hiroshi; Kaneda, Sohichi; Hama, Yoshiaki; Yamanaka, Hiroshi
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 12 p. 4533 - 4538
124-40-3
二甲胺
+
17759-15-8
→
反应条件
89966-68-7
反应条件
in water T=100°C; 20 h; sealed tube;
参考文献
Sakamoto, Takao; Yoshizawa, Hiroshi; Kaneda, Sohichi; Hama, Yoshiaki; Yamanaka, Hiroshi
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 12 p. 4533 - 4538
17759-15-8
→
反应条件
89966-86-9
反应条件
1: H2O / 20 h / 100 °C / sealed tube 2: 31 percent Spectr. / phosphoryl chloride / dioxane View Scheme
参考文献
Sakamoto, Takao; Yoshizawa, Hiroshi; Kaneda, Sohichi; Hama, Yoshiaki; Yamanaka, Hiroshi
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 12 p. 4533 - 4538
17759-15-8
→
反应条件
89966-89-2
反应条件
1: H2O / 20 h / 100 °C / sealed tube 2: 69 percent Spectr. / phosphoryl chloride / dioxane 3: 79 percent / Na / Heating View Scheme
参考文献
Sakamoto, Takao; Yoshizawa, Hiroshi; Kaneda, Sohichi; Hama, Yoshiaki; Yamanaka, Hiroshi
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 12 p. 4533 - 4538
17759-15-8
→
反应条件
89966-90-5
反应条件
1: H2O / 20 h / 100 °C / sealed tube 2: 31 percent Spectr. / phosphoryl chloride / dioxane 3: 79 percent / Na / Heating View Scheme
参考文献
Sakamoto, Takao; Yoshizawa, Hiroshi; Kaneda, Sohichi; Hama, Yoshiaki; Yamanaka, Hiroshi
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 12 p. 4533 - 4538
17759-15-8
→
反应条件
89966-93-8
反应条件
1: H2O / 20 h / 100 °C / sealed tube 2: 37 percent / phosphoryl chloride / dioxane 3: Na View Scheme
参考文献
Sakamoto, Takao; Yoshizawa, Hiroshi; Kaneda, Sohichi; Hama, Yoshiaki; Yamanaka, Hiroshi
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 12 p. 4533 - 4538
17759-15-8
→
反应条件
89966-94-9
反应条件
1: H2O / 20 h / 100 °C / sealed tube 2: 37 percent / phosphoryl chloride / dioxane 3: Na View Scheme
参考文献
Sakamoto, Takao; Yoshizawa, Hiroshi; Kaneda, Sohichi; Hama, Yoshiaki; Yamanaka, Hiroshi
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 12 p. 4533 - 4538
17759-15-8
→
反应条件
89966-99-4
反应条件
trichlorophosphate in 1,4-dioxane
参考文献
Sakamoto, Takao; Yoshizawa, Hiroshi; Kaneda, Sohichi; Hama, Yoshiaki; Yamanaka, Hiroshi
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 12 p. 4533 - 4538
17759-15-8
→
反应条件
89967-00-0
反应条件
1: H2O / 20 h / 100 °C / sealed tube 2: 37 percent / phosphoryl chloride / dioxane View Scheme
参考文献
Sakamoto, Takao; Yoshizawa, Hiroshi; Kaneda, Sohichi; Hama, Yoshiaki; Yamanaka, Hiroshi
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 12 p. 4533 - 4538
