tris-(dibenzylideneacetone)dipalladium(0); C26H25N2P; C26H24NPS; N-ethyl-N,N-diisopropylamine in tetrahydrofuran
T=120°C; Heck reaction; 4 h; Microwave irradiation; optical yield given as percent eeenantioselective reaction;
参考文献
Henriksen, Signe T.; Norrby, Per-Ola; Kaukoranta, Paeivi; Andersson, Pher G.
Journal of the American Chemical Society, 2008 , vol. 130, # 31 p. 10414 - 10421
N-ethyl-N,N-diisopropylamine; bis(dibenzylideneacetone)-palladium(0); (S)-2-[2-(diphenylphosphino)benzyl]-4-iso-propyl-4,5-dihydrooxazole in tetrahydrofuran
T=60°C; Heck reaction; 20 h; Inert atmosphere; optical yield given as percent ee;
参考文献
Henriksen, Signe T.; Norrby, Per-Ola; Kaukoranta, Paeivi; Andersson, Pher G.
Journal of the American Chemical Society, 2008 , vol. 130, # 31 p. 10414 - 10421
chiral phosphorus reagent; N-ethyl-N,N-diisopropylamine; tris(dibenzylideneacetone)dipalladium (0) in ethylene glycol dimethyl ether
T=85°C; Heck arylation reaction; Further byproducts given. Title compound not separated from byproducts;
参考文献
Andersen, Nell G.; Parvez, Masood; McDonald, Robert; Keay, Brian A.
Canadian Journal of Chemistry, 2004 , vol. 82, # 2 p. 145 - 161
