1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate; triethylamine in acetonitrile
0.0833333 h; Irradiation; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Olofsson, Kristofer; Larhed, Mats; Hallberg, Anders
Journal of Organic Chemistry, 1998 , vol. 63, # 15 p. 5076 - 5079
Herbert, John M.; Kohler, Andrew D.; Le Strat, Franck; Whitehead, David
Journal of Labelled Compounds and Radiopharmaceuticals, 2007 , vol. 50, # 5-6 p. 440 - 441
1: NBS; sulfuric acid / 6 h / 20 °C
2: 87 percent / Pd(OAc)2; AsPh3
View Scheme
参考文献
Herbert, John M.; Kohler, Andrew D.; Le Strat, Franck; Whitehead, David
Journal of Labelled Compounds and Radiopharmaceuticals, 2007 , vol. 50, # 5-6 p. 440 - 441
[Ru2(p-PriC6H4Me)2(μ-Cl)Cl]2; potassium carbonate in N,N-dimethyl-formamide
T=135°C; Heck-type olefination; 12 h;
参考文献
Na, Youngim; Park, Soyoung; Han, Soo Bong; Han, Hoon; Ko, Sangwon; Chang, Sukbok
Journal of the American Chemical Society, 2004 , vol. 126, # 1 p. 250 - 258