4-硝基苯酚三氟甲基磺酸酯合成路线 （共 131 条）
反应条件
pyridine; 1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate T=150°C; 0.333333 h; microwave irradiation;
参考文献
Lesma, Giordano; Sacchetti, Alessandro; Silvani, Alessandra
Synthesis, 2006 , # 4 p. 594 - 596
反应条件
N-ethyl-N,N-diisopropylamine; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct in water; isopropyl alcohol
T=100°C; 0.25 h; Microwave irradiation;
参考文献
Kabalka, George W.; Naravane, Abhijit; Zhao, Li Li
Tetrahedron Letters, 2007 , vol. 48, # 40 p. 7091 - 7093
反应条件
triethylamine; palladium diacetate; 2,9-dimethyl-1,10-phenanthroline in N,N-dimethyl-formamide
T=60°C; 2.5 h; Yield given. Yields of byproduct given;
参考文献
Cabri, Walter; Candiani, Ilaria; Bedeschi, Angelo; Santi, Roberto
Journal of Organic Chemistry, 1993 , vol. 58, # 26 p. 7421 - 7426
反应条件
triethylamine; palladium diacetate; 1,3-bis-(diphenylphosphino)propane in N,N-dimethyl-formamide
T=100°C; 3.5 h;
参考文献
Cabri, Walter; Candiani, Ilaria; Bedeschi, Angelo; Penco, Sergio; Santi, Roberto
Journal of Organic Chemistry, 1992 , vol. 57, # 5 p. 1481 - 1486
反应条件
triethylamine; palladium diacetate in N,N-dimethyl-formamide
T=95°C; 18 h; effect of lithium halides and tetrabutyl ammonium halides on cis/trans ratio, and ratio of α- and β-substitution products; var. solvents; other triflates; Product distribution;
参考文献
Andersson, Carl-Magnus; Hallberg, Anders
Journal of Organic Chemistry, 1988 , vol. 53, # 9 p. 2112 - 2114
反应条件
caesium carbonate; palladium diacetate; tris-(o-tolyl)phosphine in 1,4-dioxane; water
T=95°C; 4 h;
参考文献
Eisai RandD Management Co., Ltd.
Patent: EP1867650 A1, 2007 ;
Location in patent: Page/Page column 35 ;
反应条件
1,3,5,7-tetra-azatricyclo[5.1.1.13,5]decane; dnpf; bis(dibenzylideneacetone)-palladium(0) in tetrahydrofuran
T=80°C; Heck Reaction; 24 h; Inert atmosphere;
参考文献
Zou, Yinjun; Qin, Liena; Ren, Xinfeng; Lu, Yunpeng; Li, Yongxin; Zhou, Jianrong
Chemistry - A European Journal, 2013 , vol. 19, # 10 p. 3504 - 3511
反应条件
potassium phosphate; tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane
T=85°C; 2 h;
参考文献
Oh-e, Takayuki; Miyaura, Norio; Suzuki, Akira
Journal of Organic Chemistry, 1993 , vol. 58, # 8 p. 2201 - 2208
反应条件
copper(l) iodide; lithium chloride; bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran; N,N-dimethyl-formamide
T=80°C; Stille coupling; 6 h;
参考文献
Hoshino, Masahide; Degenkolb, Peter; Curran, Dennis P.
Journal of Organic Chemistry, 1997 , vol. 62, # 24 p. 8341 - 8349
反应条件
potassium phosphate; triphenylphosphine; palladium diacetate in N,N-dimethyl-formamide
T=90°C; 1 h;
参考文献
Rao, Maddali L.N.; Banerjee, Debasis; Jadhav, Deepak N.
Tetrahedron Letters, 2007 , vol. 48, # 38 p. 6644 - 6647
