4-硝基苯酚三氟甲基磺酸酯合成路线 (共 131 条)
反应条件
triethylsilane; palladium diacetate; 1,3-bis(diphenylphosphino)ferrocene in N,N-dimethyl-formamide T=60°C; 0.333333 h;
参考文献
Kotsuki; Datta; Hayakawa; Suenaga
Synthesis, 1995 , # 11 p. 1348 - 1350
反应条件
caesium carbonate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct in tetrahydrofuran; water Suzuki coupling reaction; 18 h; Heating;
参考文献
Tetrahedron, , vol. 58, # 8 p. 1465 - 1470
反应条件
in acetonitrile 24 h; Heating;
参考文献
Kotsuki; Kobayashi; Suenaga; Nishizawa
Synthesis, 1990 , # 12 p. 1145 - 1147
反应条件
1: DIPEA / Pd(PPh3)2Cl2; CuI / dimethylformamide / 48 h / 45 °C 2: aq. NaOH / diethyl ether; methanol / 18 h View Scheme
参考文献
Journal of the American Chemical Society, , vol. 129, # 31 p. 9613 - 9615
反应条件
sodium carbonate; palladium on activated charcoal in ethanol; water T=20°C; Suzuki-Miyaura coupling reaction; 24 h;
参考文献
Maegawa, Tomohiro; Kitamura, Yoshiaki; Sako, Satoko; Udzu, Takahiro; Sakurai, Ai; Tanaka, Asami; Kobayashi, Yusuke; Endo, Koichi; Bora, Utpal; Kurita, Takanori; Kozaki, Atsushi; Monguchi, Yasunari; Sajiki, Hironao
Chemistry - A European Journal, 2007 , vol. 13, # 20 p. 5937 - 5943
反应条件
sodium carbonate; palladium on activated charcoal in ethanol; water T=20°C; Suzuki-Miyaura cross-coupling; 24 h;
参考文献
Kitamura, Yoshiaki; Sakurai, Ai; Udzu, Takahiro; Maegawa, Tomohiro; Monguchi, Yasunari; Sajiki, Hironao
Tetrahedron, 2007 , vol. 63, # 43 p. 10596 - 10602
反应条件
lithium chloride; bis-triphenylphosphine-palladium(II) chloride in N,N-dimethyl-formamide T=80°C; Stille coupling; 25 h;
参考文献
Journal of Organic Chemistry, , vol. 62, # 24 p. 8341 - 8349
反应条件
potassium phosphate; triphenylphosphine; palladium diacetate in N,N-dimethyl-formamide T=90°C; 1 h;
参考文献
Rao, Maddali L.N.; Banerjee, Debasis; Jadhav, Deepak N.
Tetrahedron Letters, 2007 , vol. 48, # 38 p. 6644 - 6647
反应条件
tetrabutylammomium bromide; caesium carbonate; triphenylphosphine; palladium dichloride in N,N-dimethyl acetamide T=90°C; 1 h;
参考文献
Rao, Maddali L.N.; Jadhav, Deepak N.; Banerjee, Debasis
Tetrahedron, 2008 , vol. 64, # 24 p. 5762 - 5772
反应条件
sodium salt of phosphorous acid; palladium on activated charcoal in water; isopropyl alcohol T=20°C; Suzuki-Miyaura cross-coupling; 24 h;
参考文献
Tetrahedron, , vol. 63, # 43 p. 10596 - 10602