4-硝基苯酚三氟甲基磺酸酯合成路线 （共 131 条）
反应条件
1,3-bis-(diphenylphosphino)propane; triethylamine; palladium diacetate in N,N-dimethyl-formamide T=60°C; 40 h;
参考文献
Larhed, Mats; Andersson, Carl-Magnus; Hallberg, Anders
Tetrahedron, 1994 , vol. 50, # 2 p. 285 - 304
反应条件
1: Et3N / 1,3-bis(diphenylphosphino)propane / Pd(OAc)2 / dimethylformamide / 3.5 h / 100 °C 2: 5percent HCl / 0.5 h View Scheme
参考文献
Cabri, Walter; Candiani, Ilaria; Bedeschi, Angelo; Penco, Sergio; Santi, Roberto
Journal of Organic Chemistry, 1992 , vol. 57, # 5 p. 1481 - 1486
反应条件
oxonium; triethylamine; palladium diacetate; 2,9-dimethyl-1,10-phenanthroline 1.) DMF, 60 deg C, 2.5 h; Yield given. Multistep reaction;
参考文献
Cabri, Walter; Candiani, Ilaria; Bedeschi, Angelo; Santi, Roberto
Journal of Organic Chemistry, 1993 , vol. 58, # 26 p. 7421 - 7426
反应条件
tris(dibenzylideneacetone)dipalladium(0) chloroform complex; 1,1'-bis-(diphenylphosphino)ferrocene in various solvent(s) T=60°C; 2 h;
参考文献
Takagi, Kentaro; Sasaki, Ken; Sakakibara, Yasumasa
Bulletin of the Chemical Society of Japan, 1991 , vol. 64, # 4 p. 1118 - 1121
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate; sodium carbonate in N,N-dimethyl acetamide T=140°C; 24 h; Inert atmosphere;
参考文献
Zhu, Yi-Zhong; Cai, Chun
Synthetic Communications, 2008 , vol. 38, # 16 p. 2753 - 2760
反应条件
caesium carbonate; triphenylphosphine; palladium diacetate in toluene T=100°C;
参考文献
Advanced Synthesis and Catalysis, , vol. 347, # 2-3 p. 313 - 319
反应条件
1: dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; tripotassium phosphate monohydrate; palladium diacetate / toluene 2: 10 palladium on activated charcoal; hydrogen / ethanol View Scheme
参考文献
O'Connell, Daniel P.; Leblanc, Daniel F.; Cromley, Debra; Billheimer, Jeffrey; Rader, Daniel J.; Bachovchin, William W.
Bioorganic and Medicinal Chemistry Letters, 2012 , vol. 22, # 3 p. 1397 - 1401
反应条件
in acetonitrile T=100°C; P=7500600 Torr; 20 h;
参考文献
Kotsuki; Kobayashi; Suenaga; Nishizawa
Synthesis, 1990 , # 12 p. 1145 - 1147
反应条件
palladium diacetate; N-ethyl-N,N-diisopropylamine; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in N,N-dimethyl-formamide T=100°C; 4 h; Inert atmosphere;
参考文献
Lee, Jae-Young; Phil, Ho Lee
Journal of Organic Chemistry, 2008 , vol. 73, # 18 p. 7413 - 7416
反应条件
N-ethyl-N,N-diisopropylamine; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene; tris(dibenzylideneacetone)dipalladium (0) in 1,4-dioxane 7 h; Heating;
参考文献
BANYU PHARMACEUTICAL CO., LTD
Patent: WO2006/38741 A1, 2006 ;
Location in patent: Page/Page column 45; 61-62 ;
