4-硝基苯酚三氟甲基磺酸酯合成路线 （共 131 条）
反应条件
in acetonitrile 12 h; Heating;
参考文献
Synthesis, , # 12 p. 1145 - 1147
反应条件
triphenylphosphine; [(CO)4Fe(μ-PPh2)Pd(μ-Cl)]2 in benzene T=78°C; 1.5 h;
参考文献
Shenglof, Margarita; Gelman, Dmitri; Heymer, Bernd; Schumann, Herbert; Molander, Gary A.; Blum, Jochanan
Synthesis, 2003 , # 2 p. 302 - 306
反应条件
1.1: dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; tripotassium phosphate monohydrate; palladium diacetate / toluene 2.1: 10 palladium on activated charcoal; hydrogen / ethanol 3.1: hydrogenchloride; sodium nitrite / water / Cooling with ice 4.1: dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; palladium diacetate; triethylamine / 1,4-dioxane / 80 °C 5.1: potassium hydrogen fluoride / methanol; water / 0.5 h 5.2: 1 h View Scheme
参考文献
O'Connell, Daniel P.; Leblanc, Daniel F.; Cromley, Debra; Billheimer, Jeffrey; Rader, Daniel J.; Bachovchin, William W.
Bioorganic and Medicinal Chemistry Letters, 2012 , vol. 22, # 3 p. 1397 - 1401
反应条件
caesium carbonate in N,N-dimethyl-formamide T=100°C;
参考文献
Cui, Sun-Liang; Jiang, Zhi-Yong; Wang, Yan-Guang
Synlett, 2004 , # 10 p. 1829 - 1831
反应条件
1: dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; tripotassium phosphate monohydrate; palladium diacetate / toluene 2: 10 palladium on activated charcoal; hydrogen / ethanol 3: hydrogenchloride; sodium nitrite / water / Cooling with ice View Scheme
参考文献
O'Connell, Daniel P.; Leblanc, Daniel F.; Cromley, Debra; Billheimer, Jeffrey; Rader, Daniel J.; Bachovchin, William W.
Bioorganic and Medicinal Chemistry Letters, 2012 , vol. 22, # 3 p. 1397 - 1401
反应条件
1: dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; tripotassium phosphate monohydrate; palladium diacetate / toluene 2: 10 palladium on activated charcoal; hydrogen / ethanol 3: hydrogenchloride; sodium nitrite / water / Cooling with ice 4: dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; palladium diacetate; triethylamine / 1,4-dioxane / 80 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 22, # 3 p. 1397 - 1401
反应条件
1: tetrakis(dimethylamino)diboron With potassium acetate; 3-hydroxy-2,2-dimethylpropanol in toluene 2: 4-nitrophenyl trifluoromethanesulphonate in toluene T=80°C; 24 h;
参考文献
Tetrahedron Letters, , vol. 53, # 46 p. 6230 - 6235,6
反应条件
1: tetrakis(dimethylamino)diboron; 3-hydroxy-2,2-dimethylpropanol With potassium acetate in toluene T=80°C; 2: 4-nitrophenyl trifluoromethanesulphonate With tetrakis(triphenylphosphine) palladium(0) in toluene T=80°C; 22 h;
参考文献
Tetrahedron Letters, , vol. 53, # 46 p. 6230 - 6235,6
反应条件
1: dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; tripotassium phosphate monohydrate; palladium diacetate / toluene 2: 10 palladium on activated charcoal; hydrogen / ethanol 3: hydrogenchloride; sodium nitrite / water / Cooling with ice View Scheme
参考文献
O'Connell, Daniel P.; Leblanc, Daniel F.; Cromley, Debra; Billheimer, Jeffrey; Rader, Daniel J.; Bachovchin, William W.
Bioorganic and Medicinal Chemistry Letters, 2012 , vol. 22, # 3 p. 1397 - 1401
反应条件
potassium fluoride; 18-crown-6 ether in N,N,N',N',N'',N''-hexamethylphosphoric triamide
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 295 - 298
