177698-19-0合成路线 （共 114 条）
反应条件
1: 180 - 220 °C
2: (saponification)
View Scheme
参考文献
Watanabe,S.
Bulletin of the Chemical Society of Japan, 1965 , vol. 38, p. 1231 - 1235
反应条件
water; mercury dichloride in acetone
Ambient temperatureother mercury(II) salts ( Hg(ClO4)2, Hg(NO3)2, HgSO4); n.m.r. evidence for an intermediate organomercury(II) compound (can be reduced by NaBH4); SE2' mechanism in the conversion of intermediate into product (labelled atoms evidence); MechanismProduct distribution;
参考文献
Bluthe, Norbert; Ecoto, Jules; Fetizon, Marcel; Lazare, Sylvain
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1747 - 1751
反应条件
1: m-chloroperoxybenzoic acid / tetrahydrofuran / 3 h / 0 °C
2: Hg(ClO4)2, H2O / tetrahydrofuran / Ambient temperature; other mercury(II) salts (Hg(NO3)2, HgSO4)
View Scheme
参考文献
Bluthe, Norbert; Ecoto, Jules; Fetizon, Marcel; Lazare, Sylvain
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1747 - 1751
反应条件
4 Pd/C; hydrogen in octane
T=150°C; Autoclave;
参考文献
Deliy; Simakova
Russian Chemical Bulletin, 2008 , vol. 57, # 10 p. 2056 - 2064
反应条件
T=900°C; P=0.05 Torr; other derivatives of pinane; var. temp.; Product distribution;
参考文献
Anikeev; Ermakova; Chibiryaev; Kozhevnikov
Kinetics and Catalysis, 2010 , vol. 51, # 2 p. 162 - 193
反应条件
Pyrolysispacked quartz tube; Further byproducts given;
参考文献
Stolle, Achim; Brauns, Claudia; Nuechter, Matthias; Ondruschka, Bernd; Bonrath, Werner; Findeisen, Matthias
European Journal of Organic Chemistry, 2006 , # 15 p. 3317 - 3325
反应条件
in chloroform
T=450°C; Product distribution; Further Variations:Temperatures;
参考文献
Stolle, Achim; Ondruschka, Bernd; Bonrath, Werner
European Journal of Organic Chemistry, 2007 , # 14 p. 2310 - 2317
反应条件
in ethanol
P=91206.1 Torr; Supercritical conditionsHeating; Kinetics; PressureSolvent;
参考文献
Anikeev; Ermakova; Chibiryaev; Kozhevnikov
Kinetics and Catalysis, 2010 , vol. 51, # 2 p. 162 - 193
反应条件
5-chloro-1-methylimidazole; FeCl3·6H2O; dihydrogen peroxide in 1,1-dimethylpropan-1-ol; water
T=20°C; 1 h;
参考文献
Schroeder, Kristin; Junge, Kathrin; Spannenberg, Anke; Beller, Matthias
Catalysis Today, 2010 , vol. 157, # 1-4 p. 364 - 370
反应条件
pyridine-2,6-dicarboxylic acid; N1,N1-Dimethyl-N2-cyclohexylformamidine; dihydrogen peroxide; iron
参考文献
Schroeder, Kristin; Enthaler, Stephan; Join, Benoit; Junge, Kathrin; Beller, Matthias
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 10 p. 1771 - 1778
