piperidine in acetonitrile
HeatingSoxhlet apparatus with MgSO4;
参考文献
Bostick, Tracy Matthew; Christie, Sean D.; Connolly, Terrence Joseph; Copp, Steven; Langler, Richard Francis; Reid, Darren Leonard; Zaworotko, Michael
Australian Journal of Chemistry, 1996 , vol. 49, # 2 p. 243 - 247
Bostick, Tracy Matthew; Christie, Sean D.; Connolly, Terrence Joseph; Copp, Steven; Langler, Richard Francis; Reid, Darren Leonard; Zaworotko, Michael
Australian Journal of Chemistry, 1996 , vol. 49, # 2 p. 243 - 247
1: With [Rh(OH)(cycloocta-1,5-diene)]2; 2,2'-bis-(diphenylphosphino)-1,1'- binaphthyl in 1,4-dioxane; water
T=75°C; 14 h; Inert atmosphere;
2: With hydrogenchloride in 1,4-dioxane; water
T=75°C; 3 h;
