3-(二甲基烯丙基)吲哚合成路线 （共 20 条）
反应条件
methylmagnesium bromide; benzenesulfonyl chloride 1.) Et2O, THF, RT, 1 h, 2.) Et2O, THF, 3 h; Yield given. Multistep reaction;
参考文献
Wenkert, Ernest; Moeller, Peter D. R.; Piettre, Serge R.; McPhail, Andrew T.
Journal of Organic Chemistry, 1987 , vol. 52, # 15 p. 3404 - 3409
反应条件
potassium hydroxide; tetra(n-butyl)ammonium hydrogensulfate 1.) benzene, RT, 5 min, 2.) benzene, 0.5 h; Yield given. Multistep reaction;
参考文献
Wenkert, Ernest; Moeller, Peter D. R.; Piettre, Serge R.; McPhail, Andrew T.
Journal of Organic Chemistry, 1987 , vol. 52, # 15 p. 3404 - 3409
反应条件
ammonium hydrogen carbonate in water; acetone
T=20°C; 2 h;
参考文献
Westermaier, Martin; Mayr, Herbert
Organic Letters, 2006 , vol. 8, # 21 p. 4791 - 4794
反应条件
(η3-allyl)2Pd(cod)BF4; C21H10F12NOP in toluene
T=80°C; 24 h; Inert atmosphere;
参考文献
Usui, Ippei; Schmidt, Stefan; Keller, Manfred; Breit, Bernhard
Organic Letters, 2008 , vol. 10, # 6 p. 1207 - 1210
反应条件
zinc in tetrahydrofuran
T=20°C; Barbier reaction; 4 h;
参考文献
Yadav; Reddy; Reddy, P.Muralikrishna; Srinivas
Tetrahedron Letters, 2002 , vol. 43, # 29 p. 5185 - 5187
反应条件
ammonium hydrogen carbonate in water; acetone
T=20°C; 1 h;
参考文献
Westermaier, Martin; Mayr, Herbert
Organic Letters, 2006 , vol. 8, # 21 p. 4791 - 4794
反应条件
disodium hydrogenphosphate; sodium amalgam in methanol
1 h; Ambient temperature;
参考文献
Wenkert, Ernest; Angell, E. Charles; Ferreira, Vitor F.; Michelotti, Enrique L.; Piettre, Serge R.; et al.
Journal of Organic Chemistry, 1986 , vol. 51, # 12 p. 2343 - 2351
反应条件
1: indole With NH4PF6; 2C5H8O2*MoO2 in acetonitrile
T=65°C; 0.0833333 h;
2: 3,3-dimethylallyl alcohol in acetonitrile
T=65°C; 18 h;
参考文献
Yang, Hongwei; Fang, Ling; Zhang, Ming; Zhu, Chengjian
European Journal of Organic Chemistry, 2009 , # 5 p. 666 - 672
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
a) 0 deg C, 0.5 h, b) RT, 1 h;
参考文献
Wenkert, Ernest; Angell, E. Charles; Ferreira, Vitor F.; Michelotti, Enrique L.; Piettre, Serge R.; et al.
Journal of Organic Chemistry, 1986 , vol. 51, # 12 p. 2343 - 2351
反应条件
in chloroform
T=60°C;
参考文献
Renzi, Augusto De; Lombardi, Angelina; Panunzi, Achille; Saporito, Antonio
Gazzetta Chimica Italiana, 1988 , vol. 118, # 9 p. 657 - 660
