2-羟基-4-(甲硫基)丁腈合成路线 (共 14 条)
反应条件
sodium hydroxide; hydrogen cyanide; sulfuric acid in methanol
参考文献
Journal of the Chemical Society, , p. 1611
反应条件
1: 3-methylsulfanyl-propionaldehyde; 3-(methylseleno)-propionaldehyde With sodium hydrogensulfite in water T=20°C; 0.166667 h; 2: sodium cyanide in water T=20°C; 2 h;
参考文献
US8309763 B2, ;
Page/Page column 7 ;
反应条件
triethyl borane T=-10 - 20°C; 0.0833333 h; UV-irradiation;
参考文献
EP1260500 A1, ;
Example 10 ;
反应条件
water; sodium hydrogensulfite
参考文献
Journal of the American Chemical Society, , vol. 70, p. 1450
反应条件
water; Titanium(IV) oxide T=130°C; 5.5 h;
参考文献
DEGUSSA AG
Patent: WO2004/89863 A1, 2004 ;
Location in patent: Page column 7 ;
反应条件
1: NH3 / unter Druck 2: aqueous H2SO4 View Scheme
参考文献
Catch et al.
Journal of the Chemical Society, 1947 , p. 1611
反应条件
potassium phosphate buffer; nitrilase from Alcaligenes faecalis ATCC8750 T=30°C; pH=7.3; 48 h;
参考文献
Rey, Patrick; Rossi, Jean-Christophe; Taillades, Jacques; Gros, Georges; Nore, Olivier
Journal of Agricultural and Food Chemistry, 2004 , vol. 52, # 26 p. 8155 - 8162
反应条件
Na2B4O7; potassium cyanide in water T=80°C; 1.5 h;
参考文献
Tetrahedron Letters, , vol. 30, # 5 p. 563 - 564
参考文献
US2008/242888 A1, ;
Page/Page column 2 ;