(E)-N-(苄氧基)-1-(苯磺酰基)甲亚胺合成路线 (共 8 条)
反应条件
sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid in dichloromethane T=40°C; 2 h;
参考文献
Kim, Sunggak; Lee, Ill Young; Yoon, Joo-Yong; Oh, Dong Hyun
Journal of the American Chemical Society, 1996 , vol. 118, # 21 p. 5138 - 5139
反应条件
1: 88 percent / NCS / dimethylformamide / 3 h / 40 °C 2: 90 percent / tetrahydrofuran / 3 h / 25 °C 3: 88 percent / MCPBA, NaHCO3 / CH2Cl2 / 2 h / 40 °C View Scheme
参考文献
Kim, Sunggak; Lee, Ill Young; Yoon, Joo-Yong; Oh, Dong Hyun
Journal of the American Chemical Society, 1996 , vol. 118, # 21 p. 5138 - 5139
反应条件
1: 90 percent / tetrahydrofuran / 3 h / 25 °C 2: 88 percent / MCPBA, NaHCO3 / CH2Cl2 / 2 h / 40 °C View Scheme
参考文献
Kim, Sunggak; Lee, Ill Young; Yoon, Joo-Yong; Oh, Dong Hyun
Journal of the American Chemical Society, 1996 , vol. 118, # 21 p. 5138 - 5139
反应条件
tri-n-butyl-tin hydride in benzene T=25°C; 0.25 h; Irradiation; Rate constant;
参考文献
Kim, Sunggak; Lee, Ill Young
Tetrahedron Letters, 1998 , vol. 39, # 12 p. 1587 - 1590
反应条件
2,2'-azo-bisisobutyronitrile in benzene T=80°C; 15 h; Inert atmosphere;
参考文献
Chemistry - A European Journal, , vol. 17, # 49 p. 13904 - 13911
反应条件
2,2'-azo-bisisobutyronitrile in benzene T=80°C; 15 h; Inert atmosphere;
参考文献
Chemistry - A European Journal, , vol. 17, # 49 p. 13904 - 13911
反应条件
di-tert-butyl peroxide in tert-butyl benzene T=140°C; Inert atmosphere;
参考文献
Chemistry - A European Journal, , vol. 17, # 49 p. 13904 - 13911
反应条件
2,2'-azo-bisisobutyronitrile in benzene T=80°C; 15 h; Inert atmosphere; optical yield given as percent de;
参考文献
Chemistry - A European Journal, , vol. 17, # 49 p. 13904 - 13911