aluminium trichloride in dichloromethane added at -70 deg C, then at room temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tolstikov, G. A.; Valitov, F. Kh.; Kuchin, A. V.
J. Gen. Chem. USSR (Engl. Transl.), 1982 , vol. 52, # 6 p. 1328 - 1334,1170 - 1175
in further solvent(s) byproducts: LiCl, isobutylene; NaAlH4, dec-1-ene loaded in a vertical-type ball mill under Ar or N2; mixt. agitated for 10 min at 70°C; (i-Bu)2AlCl added for 0.5 h; mixt. stored for 1.5 h at 95-100°C; isobutylene collected in a trap cooled with liq. N2; ppt. sepd.; filtrate heated for 1 h at 80°C (1 Torr); elem. anal.;
参考文献
Russian Chemical Bulletin, , vol. 52, # 1 p. 168 - 169
