Muntyan,G.E. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1972 , vol. 21, p. 861 - 865
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1972 , vol. 21, # 4 p. 909 - 914
1: Methyltriphenylphosphonium bromide With sodium hydride in dimethyl sulfoxide
T=20°C; 1 h;
2: 3,3,5-trimethyl-cyclohexanone in dimethyl sulfoxide
T=50°C; Wittig reaction; 18 h; Further stages.;
参考文献
Weijers, Carel A. G. M.; Koenst, Paul M.; Franssen, Maurice C. R.; Sudhoelter, Ernst J. R.
Organic and Biomolecular Chemistry, 2007 , vol. 5, # 19 p. 3106 - 3114
1: Methyltriphenylphosphonium bromide With n-butyllithium in tetrahydrofuran; hexane
T=0°C; Wittig type reaction;
2: 3,5-dimethoxy-benzyl alcohol With 4,4'-di-tert-butylbiphenyl; lithium; nickel dichloride in tetrahydrofuran; hexane
Wittig type reaction; 8 h; Inert atmosphereReflux;
参考文献
Alonso, Francisco; Riente, Paola; Yus, Miguel
European Journal of Organic Chemistry, 2009 , # 34 p. 6034 - 6042