甲氧甲酰基甲基三苯基溴化膦合成路线 （共 40 条）
反应条件
n-butyllithium in tetrahydrofuran; hexane 0.5 h; Ambient temperature;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 9 p. 568 - 569
反应条件
1: 100 percent / NaOH / CH2Cl2; H2O 2: 85 percent / CH2Cl2 / 20 °C 3: 100 percent / NaOH / CH2Cl2; H2O View Scheme
参考文献
Werkhoven, Thekla M.; Van Nispen, Reinier; Lugtenburg, Johan
European Journal of Organic Chemistry, 1999 , # 11 p. 2909 - 2914
反应条件
1: NaOCH3 / CH2Cl2 / Ambient temperature 2: H2 / 5percent Pd/C / methanol / 1 h / Ambient temperature View Scheme
参考文献
Hashizume; Ito; Yamada; Nagashima; Kanao; Tomoda; Sunazuka; Kumagai; Omura
Chemical and pharmaceutical bulletin, 1994 , vol. 42, # 3 p. 512 - 520
参考文献
Castells,J. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1979 , p. 1 - 6
反应条件
1: NaOCH3 / CH2Cl2 / Ambient temperature 2: H2 / Pt/C / methanol / 1 h / Ambient temperature View Scheme
参考文献
Hashizume; Ito; Yamada; Nagashima; Kanao; Tomoda; Sunazuka; Kumagai; Omura
Chemical and pharmaceutical bulletin, 1994 , vol. 42, # 3 p. 512 - 520
反应条件
1: NaOCH3 / CH2Cl2 / Ambient temperature 2: H2 / Pt/C / methanol / 1 h / Ambient temperature 3: LiAlH4 / diethyl ether / 1 h / Heating 4: 1.) (COCl)2, DMSO, 2.) Et3N / 1.) CH2Cl2, -40 deg C, 25 min, 2.) CH2Cl2, -40 deg C, 5 min View Scheme
参考文献
Hashizume; Ito; Yamada; Nagashima; Kanao; Tomoda; Sunazuka; Kumagai; Omura
Chemical and pharmaceutical bulletin, 1994 , vol. 42, # 3 p. 512 - 520
反应条件
2: NaNH2 View Scheme
参考文献
Aitken, R. Alan; Bjornstad, Vidar; Massil, Tracy; Skramstad, Jan
Phosphorus, Sulfur and Silicon and Related Elements, 1999 , vol. 144-146, p. 577 - 580
反应条件
KBrO3; hydrogenchloride; potassium bromide
参考文献
Maerkl,G.
Chemische Berichte, 1962 , vol. 95, p. 3003 - 3007
反应条件
potassium carbonate; lithium bromide in tetrahydrofuran 6 h;
参考文献
Zhu; Kayser
Synthetic Communications, 1994 , vol. 24, # 8 p. 1179 - 1186
反应条件
sodium ethanolate 1.) ethanol, 2.) ethanol, reflux, 10 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Ganoub, Neven A. F.
Phosphorus, Sulfur and Silicon and the Related Elements, 1993 , vol. 81, # 1-4 p. 125 - 132
