甲氧甲酰基甲基三苯基溴化膦合成路线 （共 40 条）
反应条件
sodium hydroxide in ethylene glycol dimethyl ether; pentane
2 h; Ambient temperature;
参考文献
Suzuki, Toshio; Sato, Etsuko; Kamada, Shinko; Tada, Hitoshi; Unno, Katsuo; Kametani, Tetsuii
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 387 - 392
反应条件
sodium hydroxide in ethylene glycol dimethyl ether; pentane
2 h; Ambient temperature;
参考文献
Suzuki, Toshio; Sato, Etsuko; Kamada, Shinko; Tada, Hitoshi; Unno, Katsuo; Kametani, Tetsuii
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 387 - 392
反应条件
1: NaOCH3 / CH2Cl2 / Ambient temperature
2: H2 / 5percent Pd/C / methanol / 1 h / Ambient temperature
3: LiAlH4 / diethyl ether / 1 h / Heating
4: 1.) (COCl)2, DMSO, 2.) Et3N / 1.) CH2Cl2, -40 deg C, 25 min, 2.) CH2Cl2, -40 deg C, 5 min
View Scheme
参考文献
Hashizume; Ito; Yamada; Nagashima; Kanao; Tomoda; Sunazuka; Kumagai; Omura
Chemical and pharmaceutical bulletin, 1994 , vol. 42, # 3 p. 512 - 520
反应条件
triethylamine
1.) THF, 24 h, room t., 2.) THF, 24 h; Yield given. Multistep reaction;
参考文献
Franzen, Robert
Tetrahedron Letters, 1995 , vol. 36, # 22 p. 3905 - 3908
反应条件
triethylamine
1.) THF, 24 h, room t., 2.) THF, 24 h; Yield given. Multistep reaction;
参考文献
Franzen, Robert
Tetrahedron Letters, 1995 , vol. 36, # 22 p. 3905 - 3908
反应条件
triethylamine
1.) THF, 24 h, room t., 2.) THF, 24 h; Yield given. Multistep reaction;
参考文献
Franzen, Robert
Tetrahedron Letters, 1995 , vol. 36, # 22 p. 3905 - 3908
反应条件
triethylamine
multistep reaction: 1.) THF, 24 h, room t., 2.) THF, 24 h reactions with var. chlorinated propanones under var. conditions; Product distributionMechanism;
参考文献
Franzen, Robert
Tetrahedron Letters, 1995 , vol. 36, # 22 p. 3905 - 3908
反应条件
1: Br2, NaOAc / acetic acid
2: Br2 / CHCl3
3: acetonitrile
View Scheme
参考文献
Maerkl,G.
Chemische Berichte, 1962 , vol. 95, p. 3003 - 3007
反应条件
1: 100 percent / NaOH / CH2Cl2; H2O
2: 85 percent / CH2Cl2 / 20 °C
View Scheme
参考文献
Werkhoven, Thekla M.; Van Nispen, Reinier; Lugtenburg, Johan
European Journal of Organic Chemistry, 1999 , # 11 p. 2909 - 2914
反应条件
sodium carbonate in diethyl ether; hexane
T=35°C; Wittig olefination; 1.5 h; sonification;
参考文献
Watanabe, Masataka; Morais, Goreti Ribeiro; Mataka, Shuntaro; Ideta, Keiko; Thiemann, Thies
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 2005 , vol. 60, # 8 p. 909 - 915
