4-溴-3-氧代-丁酸甲酯合成路线 (共 15 条)
参考文献
Cheruku, Pradeep; Paptchikhine, Alexander; Ali, Muhammad; Neudoerfl, Joerg-M.; Andersson, Pher G.
Organic and Biomolecular Chemistry, 2008 , vol. 6, # 2 p. 366 - 373
反应条件
chloro-trimethyl-silane T=20°C; 24 h;
参考文献
Zav'yalev, S. I.; Zavozin, A. G.; Kravchenko, N. E.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1991 , vol. 40, # 5.2 p. 1104 - 1106
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1991 , vol. 40, # 5 p. 1227 - 1229
反应条件
chloro-trimethyl-silane; bromine T=20°C; 24 h;
参考文献
Zav'yalev, S. I.; Zavozin, A. G.; Kravchenko, N. E.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1991 , vol. 40, # 5.2 p. 1104 - 1106
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1991 , vol. 40, # 5 p. 1227 - 1229
反应条件
iso-propylmagnesium bromide in diethyl ether
参考文献
Kel'in, A. V.; Kulinkovich, O. G.
Russian Journal of Organic Chemistry, 1994 , vol. 30, # 7.2 p. 1129 - 1130
Zhurnal Organicheskoi Khimii, 1994 , vol. 30, # 7 p. 1070 - 1071
参考文献
Chan,T.H.; Brownbridge,P.
Journal of the Chemical Society, Chemical Communications, 1979 , p. 578 - 579
反应条件
1: (i) LDA, TMEDA, THF, (ii) /BRN= 1209232/ 2: Br2 View Scheme
参考文献
Chan,T.H.; Brownbridge,P.
Journal of the Chemical Society, Chemical Communications, 1979 , p. 578 - 579
反应条件
bromine 1.) CCl4, 5 min, 2.) CCl4, 10 min; Yield given. Multistep reaction;
参考文献
Wolfe; Jin; Yang; Kim; McEachern
Canadian Journal of Chemistry, 1994 , vol. 72, # 4 p. 1051 - 1065
参考文献
Yuan, Chengye; Wang, Ke; Li, Jinfeng; Li, Zuyi
Heteroatom Chemistry, 2002 , vol. 13, # 2 p. 153 - 156
反应条件
in methanol 0.166667 h; Heating;
参考文献
Simoneau, Bruno; Brassard, Paul
Tetrahedron, 1986 , vol. 42, # 14 p. 3767 - 3774
反应条件
piperidine in dichloromethane; acetic acid T=-29 - -25°C; 4 h;
参考文献
Sumitomo Chemical Co., Ltd.; Shionogi and Co., Ltd.
Patent: US6340763 B1, 2002 ;
Location in patent: Page column 16 ;