4,4,5,5-四甲基-2-(3-苯氧基丙基)-1,3,2-二噁硼烷合成路线 （共 6 条）
反应条件
terpyridine; [RhCl(η2:η2-cycloocta-1,5-diene)]2; sodium t-butanolate T=80°C; 24 h; Inert atmosphere;
参考文献
Gong, Tian-Jun; Jiang, Yuan-Ye; Fu, Yao
Chinese Chemical Letters, 2014 , vol. 25, # 3 p. 397 - 400
反应条件
di-μ-chloro-bis(η4-1,5-cyclooctadiene)diiridium; bis(1,1-diphenylphosphino)methane in dichloromethane T=20°C; 24 h;
参考文献
Yamamoto, Yasunori; Fujikawa, Rhyou; Umemoto, Tomokazu; Miyaura, Norio
Tetrahedron, 2004 , vol. 60, # 47 p. 10695 - 10700
反应条件
tris-(dibenzylideneacetone)dipalladium(0); P(t-Bu)2Me*HBF4; sodium methylate in 1,4-dioxane T=25°C; 24 h; Inert atmosphere;
参考文献
Yi, Jun; Liu, Jin-Hui; Liang, Jun; Dai, Jian-Jun; Yang, Chu-Ting; Fu, Yao; Liu, Lei
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 9 p. 1685 - 1691
反应条件
1.1: sodium periodate / water; tetrahydrofuran / 0.08 h 1.2: 20 °C 2.1: 1,10-phenanthroline; silver carbonate; potassium phosphate; copper(l) iodide; silver fluoride / N,N-dimethyl-formamide / 24 h / 80 °C / |Glovebox; |Inert atmosphere View Scheme
参考文献
Xu, Jun; Xiao, Bin; Xie, Chuan-Qi; Luo, Dong-Fen; Liu, Lei; Fu, Yao
Angewandte Chemie - International Edition, 2012 , vol. 51, # 50 p. 12551 - 12554
Angew. Chem., 2012 , vol. 124, # 50 p. 12719 - 12722,4
反应条件
1.1: sodium periodate / water; tetrahydrofuran / 0.08 h 1.2: 20 °C 2.1: 1,10-phenanthroline; copper(I) thiophene-2-carboxylate; silver carbonate; potassium phosphate; silver fluoride / N,N-dimethyl-formamide / 24 h / 80 °C / |Glovebox; |Inert atmosphere View Scheme
参考文献
Xu, Jun; Xiao, Bin; Xie, Chuan-Qi; Luo, Dong-Fen; Liu, Lei; Fu, Yao
Angewandte Chemie - International Edition, 2012 , vol. 51, # 50 p. 12551 - 12554
Angew. Chem., 2012 , vol. 124, # 50 p. 12719 - 12722,4
反应条件
1.1: sodium periodate / water; tetrahydrofuran / 0.08 h 1.2: 20 °C 2.1: 1,10-phenanthroline; copper(I) thiophene-2-carboxylate; silver carbonate; potassium phosphate; silver fluoride / N,N-dimethyl-formamide / 24 h / 80 °C / |Glovebox; |Inert atmosphere View Scheme
参考文献
Xu, Jun; Xiao, Bin; Xie, Chuan-Qi; Luo, Dong-Fen; Liu, Lei; Fu, Yao
Angewandte Chemie - International Edition, 2012 , vol. 51, # 50 p. 12551 - 12554
Angew. Chem., 2012 , vol. 124, # 50 p. 12719 - 12722,4
