1-(4-氯苯基)-1-甲基乙基胺合成路线 （共 7 条）
反应条件
T=-78 - 0°C; 2 h; 5.0 equival. MeCeCl2;
参考文献
Calderwood, David J.; Davies, Roy V.; Rafferty, Paul; Twigger, Helen L.; Whelan, Helen M.
Tetrahedron Letters, 1997 , vol. 38, # 7 p. 1241 - 1244
反应条件
hydrogen; Lindlar's catalyst in ethanol
参考文献
Chemistry - A European Journal, , vol. 13, # 33 p. 9207 - 9215
反应条件
aluminium trichloride; nitrogen trichloride; 1-bromo-1,1-dimethylethane in 1,2-dichloro-ethane
参考文献
Journal of Organic Chemistry, , vol. 33, p. 4515 - 4520
反应条件
T=-78 - 0°C; 2 h; 5.0 equival. MeCeCl2;
参考文献
Calderwood, David J.; Davies, Roy V.; Rafferty, Paul; Twigger, Helen L.; Whelan, Helen M.
Tetrahedron Letters, 1997 , vol. 38, # 7 p. 1241 - 1244
反应条件
hydrogenchloride in water 70-80 deg C, 0.5 h; reflux, 0.5 h;
参考文献
Agricultural and Biological Chemistry, , vol. 49, # 12 p. 3563 - 3568
反应条件
1: 1.) SOCl2; 2.) HCl gas, 3.) ZnCl2 / 1.) pyridine 2: 8N hydrochloric acid / H2O / 70-80 deg C, 0.5 h; reflux, 0.5 h View Scheme
参考文献
Agricultural and Biological Chemistry, , vol. 49, # 12 p. 3563 - 3568
反应条件
1: tetrahydrofuran 2: 1.) SOCl2; 2.) HCl gas, 3.) ZnCl2 / 1.) pyridine 3: 8N hydrochloric acid / H2O / 70-80 deg C, 0.5 h; reflux, 0.5 h View Scheme
参考文献
Agricultural and Biological Chemistry, , vol. 49, # 12 p. 3563 - 3568
