1,2,3,4-四氢-2-甲基喹啉合成路线 (共 73 条)
反应条件
(7,8-benzoquinolinato)hydrido(aqua)bis(triphenylphosphine)iridium(III) tetrakis[3,5-bis(trifluoromethyl)phenyl]borate; hydrogen in toluene T=80°C; 18 h;
参考文献
Organometallics, , vol. 32, # 16 p. 4501 - 4506
反应条件
(7,8-benzoquinolinato)hydrido(aqua)bis(triphenylphosphine)iridium(III) tetrakis[3,5-bis(trifluoromethyl)phenyl]borate; hydrogen in toluene T=80°C; 18 h;
参考文献
Organometallics, , vol. 32, # 16 p. 4501 - 4506
反应条件
N,N-dicyclohexylmethylamine; palladium diacetate; Azobenzene; P(t-Bu)2(2'-methylbiphenyl-2-yl) in acetonitrile T=90°C; Improved Larock synthesis; 14 h; Inert atmosphere;
参考文献
Stone, Matthew T.
Organic Letters, 2011 , vol. 13, # 9 p. 2326 - 2329
反应条件
palladium 10 on activated carbon; zinc T=150°C; 40 h; Autoclave;
参考文献
Organic and Biomolecular Chemistry, , vol. 10, # 9 p. 1826 - 1833
反应条件
(7,8-benzoquinolinato)hydrido(aqua)bis(triphenylphosphine)iridium(III) tetrakis[3,5-bis(trifluoromethyl)phenyl]borate; hydrogen in toluene T=80°C; 18 h;
参考文献
Organometallics, , vol. 32, # 16 p. 4501 - 4506
反应条件
aluminium trichloride in dichloromethane 6 h; Ambient temperature;
参考文献
Kawase; Kikugawa
Chemical and Pharmaceutical Bulletin, 1981 , vol. 29, # 6 p. 1615 - 1623
反应条件
(7,8-benzoquinolinato)hydrido(aqua)bis(triphenylphosphine)iridium(III) tetrakis[3,5-bis(trifluoromethyl)phenyl]borate; hydrogen in toluene T=80°C; 18 h;
参考文献
Organometallics, , vol. 32, # 16 p. 4501 - 4506
反应条件
di-μ-chloro-bis(η4-1,5-cyclooctadiene)diiridium; hydrogen; iodine; (R)-Segphos® in isopropyl alcohol; toluene T=20°C; P=37503.8 Torr; 17 h; Autoclave; Reagent/catalyst; Optical yield = 79 percent ee;
参考文献
Tetrahedron, , vol. 69, # 44 p. 9322 - 9328
反应条件
hydrogen; aluminum oxide; ruthenium in various solvent(s) T=160°C; P=38786.1 Torr; 1.6 h; Product distribution;
参考文献
Journal of Heterocyclic Chemistry, , vol. 24, p. 1477 - 1483
反应条件
aluminium trichloride in dichloromethane 6 h; Ambient temperature;
参考文献
Kawase; Kikugawa
Chemical and Pharmaceutical Bulletin, 1981 , vol. 29, # 6 p. 1615 - 1623