1,2,3,4-四氢-2-甲基喹啉合成路线 （共 73 条）
反应条件
triethylsilane; boron trifluoride diethyl etherate in dichloromethane T=100°C; 24 h;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 9, # 7 p. 1008 - 1012
反应条件
1.1: n-BuLi / tetrahydrofuran; hexane / 13 h / -70 - 0 °C 1.2: 36 percent / HCl / H2O; methanol / 29 h / 20 °C 2.1: 83 percent / potassium carbonate; [(C5Me5)IrCl2]2 / toluene / 20 h / 111 °C View Scheme
参考文献
Organic Letters, , vol. 4, # 16 p. 2691 - 2694
反应条件
(7,8-benzoquinolinato)hydrido(aqua)bis(triphenylphosphine)iridium(III) tetrakis[3,5-bis(trifluoromethyl)phenyl]borate; hydrogen in toluene T=80°C; 18 h;
参考文献
Organometallics, , vol. 32, # 16 p. 4501 - 4506
反应条件
1: 87 percent / diethyl ether / 0.03 h 2: methanol / HCl View Scheme
参考文献
Canadian Journal of Chemistry, , vol. 63, p. 412 - 417
反应条件
1: methanol / HCl / Ambient temperature; also with 2-methyl and 2-phenyl derivatives 2: 87 percent / diethyl ether / 0.03 h 3: methanol / HCl View Scheme
参考文献
Canadian Journal of Chemistry, , vol. 63, p. 412 - 417
反应条件
[Ir(η5-C5Me5)(C6H4-2-C3H5N2)(NCCH3)](PF6) in N-dodecane; toluene T=100°C; 16 h; Inert atmosphere;
参考文献
Chemistry - A European Journal, , vol. 15, # 46 p. 12780 - 12790
反应条件
aluminium trichloride in dichloromethane 6 h; Ambient temperature;
参考文献
Kawase; Kikugawa
Chemical and Pharmaceutical Bulletin, 1981 , vol. 29, # 6 p. 1615 - 1623
反应条件
lithium in tetrahydrofuran 96 h;
参考文献
Journal of Organic Chemistry, , vol. 58, # 7 p. 1926 - 1931
反应条件
trifluoroacetic acid 15 h; Heating;
参考文献
Kawase; Kikugawa
Chemical and Pharmaceutical Bulletin, 1981 , vol. 29, # 6 p. 1615 - 1623
反应条件
1: cerium ammonium nitrate / acetonitrile / 1 h / 20 °C 2: hydrochloric acid / acetonitrile; H2O / 2 h / Heating View Scheme
参考文献
Tetrahedron, , vol. 63, # 3 p. 673 - 681
