3,3-二甲基戊二酸二乙酯合成路线 （共 21 条）
反应条件
1: 79 percent / sodium / toluene / 28 h 2: 87 percent / 85 percent phosphoric acid / Heating View Scheme
参考文献
Holder, Richard W.; Daub, John P.; Baker, Wesley E.; Gilbert, Raymond H; Graf, Norman A.
Journal of Organic Chemistry, 1982 , vol. 47, # 8 p. 1445 - 1451
反应条件
1: (i) Li, (ii) /BRN= 1781737/, (heating)
2: Al2O3 / 180 °C
View Scheme
参考文献
Zimmerman,H.E.; Mariano,P.S.
Journal of the American Chemical Society, 1969 , vol. 91, # 7 p. 1718 - 1727
反应条件
1: 79 percent / sodium / toluene / 28 h
2: 87 percent / 85 percent phosphoric acid / Heating
3: 79 percent / LiAlH4 / diethyl ether / 22 h / Heating
View Scheme
参考文献
Holder, Richard W.; Daub, John P.; Baker, Wesley E.; Gilbert, Raymond H; Graf, Norman A.
Journal of Organic Chemistry, 1982 , vol. 47, # 8 p. 1445 - 1451
反应条件
1: (i) NaH, (ii) /BRN= 1781737/
2: aq. HCl, AcOH
3: H2SO4
4: NaOtBu
View Scheme
参考文献
Beringer,F.M. et al.
Tetrahedron, 1960 , vol. 8, p. 49 - 63
参考文献
Kon
Journal of the Chemical Society, 1922 , vol. 121, p. 523
参考文献
Stetter; Krause
Chemische Berichte, 1954 , vol. 87, p. 209
参考文献
Handley,G.J. et al.
Australian Journal of Chemistry, 1960 , vol. 13, p. 129 - 144
反应条件
thionyl chloride in water
参考文献
Merck and Co., Inc.
Patent: US4262010 A1, 1981 ;
反应条件
thionyl chloride in water
参考文献
Merck and Co., Inc.
Patent: US4994568 A1, 1991 ;
反应条件
1: lithium alanate; diethyl ether
2: phosphorus (III)-bromide
View Scheme
参考文献
Reid; Gompf
Journal of Organic Chemistry, 1953 , vol. 18, p. 661
Full Text View citing articles Show Details
Sorm et al.
Collection of Czechoslovak Chemical Communications, 1954 , vol. 19, p. 570,577
