2-二苯基膦-1-萘甲酸甲酯合成路线 （共 6 条）
反应条件
zinc; Cl2Ni(1,2-bis(diphenylphosphino)ethane) in N,N-dimethyl-formamide T=100 - 110°C;
参考文献
Ager, David J.; East, Michael B.; Eisenstadt, Amihai; Laneman, Scott A.
Chemical Communications, 1997 , # 24 p. 2359 - 2360
反应条件
bis(benzonitrile)palladium(II) dichloride in toluene Substitution; 26 h; Heating;
参考文献
Trost, Barry M.; Bunt, Richard C.; Lemoine, Remy C.; Calkins, Trevor L.
Journal of the American Chemical Society, 2000 , vol. 122, # 25 p. 5968 - 5976
反应条件
1: 89 percent / pyridine / CH2Cl2 / 14 h / 0 °C 2: 95 percent / bis(benzonitrile)palladium dichloride / toluene / 26 h / Heating View Scheme
参考文献
Trost, Barry M.; Bunt, Richard C.; Lemoine, Remy C.; Calkins, Trevor L.
Journal of the American Chemical Society, 2000 , vol. 122, # 25 p. 5968 - 5976
反应条件
in N,N-dimethyl-formamide
参考文献
Monsanto Company
Patent: US5874628 A1, 1999 ;
反应条件
Ba(OH)2*8H2O in methanol Hydrolysis; 25 h; Heating;
参考文献
Trost, Barry M.; Bunt, Richard C.; Lemoine, Remy C.; Calkins, Trevor L.
Journal of the American Chemical Society, 2000 , vol. 122, # 25 p. 5968 - 5976
反应条件
1.1: 88 percent / barium hydroxide octahydrate / methanol / 25 h / Heating 2.1: Et3N; diphenylchlorophosphite / CH2Cl2 / 5 h / 0 - 20 °C 2.2: 51 percent / DMAP / CH2Cl2 / 12 h / 25 °C View Scheme
参考文献
Trost, Barry M.; Bunt, Richard C.; Lemoine, Remy C.; Calkins, Trevor L.
Journal of the American Chemical Society, 2000 , vol. 122, # 25 p. 5968 - 5976
