5-氟苯-[2,1,3]-噻重氮合成路线 （共 2 条）
反应条件
thionyl chloride; triethylamine in toluene RefluxCooling;
参考文献
Albrecht, Steve; Janietz, Silvia; Schindler, Wolfram; Frisch, Johannes; Kurpiers, Jona; Kniepert, Juliane; Inal, Sahika; Pingel, Patrick; Fostiropoulos, Konstantinos; Koch, Norbert; Neher, Dieter
Journal of the American Chemical Society, 2012 , vol. 134, # 36 p. 14932 - 14944
反应条件
1: 5 Pd/C; hydrazine hydrate / ethanol / 0.5 h / -10 - 20 °C / |Inert atmosphere 2: triethylamine; thionyl chloride / chloroform / 5 h / 0 °C / |Inert atmosphere; |Reflux View Scheme
参考文献
Chemistry--A European Journal, , vol. 18, # 36 p. 11433 - 11439,7
Chemistry - A European Journal, , vol. 18, # 36 p. 11433 - 11439
