4-氨基-2,3,5,6-四氟苯甲腈合成路线 (共 8 条)
反应条件
cesium fluoride; 1,1,1,3,3,3-hexamethyl-disilazane in N,N-dimethyl-formamide T=100°C; 5 h; Yield given;
参考文献
Miller, Alexey O.; Furin, Georgii G.
Journal of Fluorine Chemistry, 1995 , vol. 75, # 2 p. 169 - 172
反应条件
ammonia in water; ethyl acetate T=20°C; 6 h;
参考文献
Wasa, Masayuki; Engle, Keary M.; Lin, David W.; Yoo, Eun Jeong; Yu, Jin-Quan
Journal of the American Chemical Society, 2011 , vol. 133, # 49 p. 19598 - 19601
反应条件
1,1,1-trimethyl-N,N-bis(trimethylsilyl)stannanamine; cesium fluoride in N,N-dimethyl-formamide Heating; Yields of byproduct given;
参考文献
Miller, Alexey O.; Furin, Georgii G.
Journal of Fluorine Chemistry, 1995 , vol. 75, # 2 p. 169 - 172
反应条件
Irradiation; Quantum yieldProduct distribution;
参考文献
Pandurangi, Raghoottama S.; Katti, Kattesh V.; Barnes, Charles L.; Volkert, Wynn A.; Kuntz, Robert R.
Journal of the Chemical Society, Chemical Communications, 1994 , # 16 p. 1841 - 1842
参考文献
Gmelin Handbook: F: PerFHalOrg.7, 1, page 1 - 84
反应条件
RuCl2(η6-C6Me6)(PTA-Bn); water T=100°C; 3 h; Inert atmosphereNeutral aq. solution; chemoselective reaction;
参考文献
Cadierno, Victorio; Francos, Javier; Gimeno, Jose
Chemistry - A European Journal, 2008 , vol. 14, # 22 p. 6601 - 6605
反应条件
sodium nitrite react with NaNO2 45 min, then in HF at 0°C, adding to soln. of CuBr in 48percent HBr at 0°C, 3 h;
参考文献
Gmelin Handbook: F: PerFHalOrg.9, 7, page 50 - 101
反应条件
diisobutylaluminium hydride in benzene 10 h;
参考文献
Kanakarajan, K.; Haider, Karl; Czarnik, Anthony W.
Synthesis, 1988 , # 7 p. 566 - 568