3,4,5,6-四氯吡啶氰合成路线 (共 8 条)
反应条件
lithium chloride in dimethyl sulfoxide T=120 - 135°C; 1.25 h;
参考文献
US2012/190857 A1, ;
Page/Page column 7 ;
反应条件
in (2S)-N-methyl-1-phenylpropan-2-amine hydrate; dimethyl sulfoxide
反应条件
chlorine in tetrachloromethane T=630°C; 0.00138889 h; var. contact times, temperatures, and solvent systems; Product distribution;
参考文献
J. Appl. Chem. USSR (Engl. Transl.), , vol. 64, # 6.2 p. 1297 - 1301,1155 - 1159
反应条件
ammonia in dimethyl sulfoxide T=50°C;
参考文献
Ovchinnikov, V.G.; Nasyr, I.A.; Litvinenko, G.S.; Maksimeno, N.M.; Zatsarevnyi, V.M.
J. Appl. Chem. USSR (Engl. Transl.), 1991 , vol. 64, # 12 p. 2490 - 2497,2327 - 2334
反应条件
ammonia T=100°C; 10 h;
参考文献
Ovchinnikov, V.G.; Nasyr, I.A.; Litvinenko, G.S.; Maksimeno, N.M.; Zatsarevnyi, V.M.
J. Appl. Chem. USSR (Engl. Transl.), 1991 , vol. 64, # 12 p. 2490 - 2497,2327 - 2334
参考文献
The Dow Chemical Company
Patent: US4336384 A1, 1982 ;
反应条件
triethylamine; hydrazine in ice-water; ethanol
参考文献
The Dow Chemical Company
Patent: US4087431 A1, 1978 ;
反应条件
potassium carbonate; cesium fluoride
T=55 - 74°C; 4.25 h; Inert atmosphere;
参考文献
DOW AGROSCIENCES LLC
Patent: US2012/190857 A1, 2012 ;
Location in patent: Page/Page column 6-7 ;