N,N-二甲基-N'-苯基甲脒合成路线 （共 39 条）
反应条件
1: in diethyl ether
T=20°C; Inert atmosphere;
2: With sodium carbonate in diethyl ether
T=20°C; Inert atmosphere;
参考文献
Chakraborty, Bhaskar; Chhetri, Manjit Singh; Kafley, Saurav; Sharma, Prawin; Rai, Neelam
Journal of the Indian Chemical Society, 2010 , vol. 87, # 11 p. 1399 - 1402
反应条件
in toluene
T=110°C; 96 h;
参考文献
Croce, Piero Dalla; Ferraccioli, Raffaella; Rosa, Concetta La
Heterocycles, 1997 , vol. 45, # 7 p. 1309 - 1318
反应条件
phenyl silane; tris[2-(diphenylphosphino)ethyl]phosphine; Fe(II) acetylacetonate in tetrahydrofuran
T=100°C; 24 h;
参考文献
Pouessel, Jacky; Jacquet, Olivier; Cantat, Thibault
ChemCatChem, 2013 , vol. 5, # 12 p. 3552 - 3556
反应条件
in toluene
T=110°C; 96 h;
参考文献
Croce, Piero Dalla; Ferraccioli, Raffaella; Rosa, Concetta La
Heterocycles, 1997 , vol. 45, # 7 p. 1309 - 1318
反应条件
in toluene
3 h; Heating;
参考文献
Tisler, Miha; Stanovnik, Branko; Zrimsek, Zdenka; Stropnik, Crtomir
Synthesis, 1981 , # 4 p. 299 - 300
反应条件
1: N,N-dimethyl-formamide With trichlorophosphate in diethyl ether
T=10 - 20°C; Inert atmosphere;
2: aniline in diethyl ether
T=10 - 20°C;
参考文献
Schroeder, Kristin; Enthaler, Stephan; Join, Benoit; Junge, Kathrin; Beller, Matthias
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 10 p. 1771 - 1778
反应条件
in water
Ambient temperature;
参考文献
Cereda, Enzo; Bellora, Elio; Donetti, Arturo
Synthesis, 1986 , # 4 p. 288 - 291
反应条件
in toluene
T=110°C; 96 h;
参考文献
Croce, Piero Dalla; Ferraccioli, Raffaella; Rosa, Concetta La
Heterocycles, 1997 , vol. 45, # 7 p. 1309 - 1318
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide
T=120°C;
参考文献
Perregaard,J. et al.
Bulletin des Societes Chimiques Belges, 1977 , vol. 86, p. 321 - 328
参考文献
Kantlehner, Willi; Wagner, Fritz; Bredereck, Hellmut
Liebigs Annalen der Chemie, 1980 , # 3 p. 344 - 357
