4-氯-2H-色烯-2-酮合成路线 （共 25 条）
反应条件
bis[2-(diphenylphosphino)phenyl] ether; potassium iodide; zinc; NiCl2((PPh3)P)2 in 1,4-dioxane T=130°C; Ullmann-type reaction; 0.5 h; microwave irradiation;
参考文献
Hashim, Jamshed; Kappe, C. Oliver
Advanced Synthesis and Catalysis, 2007 , vol. 349, # 14-15 p. 2353 - 2360
反应条件
1: 70 percent / diethyl ether; tetrahydrofuran / 1 h / 0 °C
2: 2.) H2O / 1.) hexane, ether, RT, 1 h
View Scheme
参考文献
Alberola, Angel; Calvo, Blanca; Gonzalez-Ortega, Alfonso; Lopez, Cristina; Villafane, Fernando
Heterocycles, 1994 , vol. 38, # 4 p. 819 - 832
反应条件
1: pyridine
2: (i) H2SO4, (ii) H2O
3: aq. HCl / aq. ethanol / Heating
View Scheme
参考文献
Checchi,S. et al.
Gazzetta Chimica Italiana, 1969 , vol. 99, p. 501 - 513
反应条件
bis(tri-o-tolylphosphine) palladium(II) chloride; sodium carbonate in tetrahydrofuran
Suzuki-Miyaura Coupling; 24 h; RefluxSchlenk technique;
参考文献
Shah, Parin; Santana, M. Dolores; Garcia, Joaquin; Serrano, J. Luis; Naik, Minal; Pednekar, Suhas; Kapdi, Anant R.
Tetrahedron, 2013 , vol. 69, # 5 p. 1446 - 1453
参考文献
Checchi,S. et al.
Gazzetta Chimica Italiana, 1969 , vol. 99, p. 501 - 513
