萘-1,2,4-三基三乙酸酯合成路线 （共 39 条）
反应条件
1: aq.-ethanolic NaOH / und Erwaermen der mit wss.HCl angesaeuerten Reaktionsloesung mit FeCl3 in wss.HCl 2: /BRN= 3334450/ View Scheme
参考文献
Fieser et al.
Journal of the American Chemical Society, 1948 , vol. 70, p. 3177
反应条件
1: alcohol; hydrochloric acid 2: ice; sulfuric acid; dichromate / 0 °C 3: zinc chloride View Scheme
参考文献
Thiele; Winter
Justus Liebigs Annalen der Chemie, 1900 , vol. 311, p. 355
Chem. Zentralbl., 1901 , vol. 72, # II p. 70
反应条件
bismuth trifluoromethanesulphonate in acetonitrile
T=20°C; Thiele-Winter acetoxylation; 0.75 h;
参考文献
Yadav; Reddy, B. V. Subba; Swamy; Rao, K. Raghavender
Tetrahedron Letters, 2004 , vol. 45, # 31 p. 6037 - 6039
反应条件
sulfuric acid
T=50°C; 2 h;
参考文献
Matsumoto, Takashi; Imai, Sachihiko; Yamamoto, Naoya
Bulletin of the Chemical Society of Japan, 1988 , vol. 61, p. 911 - 920
反应条件
sulfuric acid
T=50°C; 2 h;
参考文献
Matsumoto, Takashi; Imai, Sachihiko; Yamamoto, Naoya
Bulletin of the Chemical Society of Japan, 1988 , vol. 61, p. 911 - 920
反应条件
sodium acetate; zinc
参考文献
Fieser; Dunn
Journal of the American Chemical Society, 1937 , vol. 59, p. 1024,1027
反应条件
1: 2.8 percent / CH2Cl2 / 24 h / Ambient temperature
2: 90 percent / H2SO4 / 2 h / 50 °C
View Scheme
参考文献
Matsumoto, Takashi; Imai, Sachihiko; Yamamoto, Naoya
Bulletin of the Chemical Society of Japan, 1988 , vol. 61, p. 911 - 920
反应条件
1: 6 percent / CH2Cl2 / 48 h / Ambient temperature
2: 73.3 percent / H2SO4 / 2 h / 50 °C
View Scheme
参考文献
Matsumoto, Takashi; Imai, Sachihiko; Yamamoto, Naoya
Bulletin of the Chemical Society of Japan, 1988 , vol. 61, p. 911 - 920
反应条件
sulfuric acid
T=30 - 40°C;
参考文献
Bayer and Co.
Patent: DE101607 ;
Full Text Show Details
Thiele; Winter
Justus Liebigs Annalen der Chemie, 1900 , vol. 311, p. 355
Chem. Zentralbl., 1901 , vol. 72, # II p. 70
参考文献
Tommasi
Gazzetta Chimica Italiana, 1920 , vol. 50 I, p. 268
