in neat (no solvent) NO2 added to Sb deriv. at -196°C (dry box, vacuum line) and warm slowly to room temp.; volatiles pumped off; detd. by vibrational spectroscopy;
参考文献
Journal of the American Chemical Society, , vol. 123, # 26 p. 6308 - 6313
in nitromethane room temp., traces of H2O in nitromethane; N2O was detected by MS, HNO3 was detected by (14)N NMR;
参考文献
Bhasin, Kuldip K.; Crawford, Margaret-Jane; Jenkins, H. Donald Brooke; Klapoetke, Thomas M.; Liebman, Joel F.
Zeitschrift fur Anorganische und Allgemeine Chemie, 2006 , vol. 632, # 5 p. 897 - 900
