6-乙氧基-1-(4-戊烯-1-基)-2-哌啶酮合成路线 （共 4 条）
反应条件
hydrogenchloride; sodium tetrahydroborate T=-10°C; Reduction; 2 h;
参考文献
Tarling, Chris A.; Holmes, Andrew B.; Markwell, Roger E.; Pearson, Neil D.
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 12 p. 1695 - 1701
反应条件
1: 66 percent / PPh3, DEAD / tetrahydrofuran / 24 h / Ambient temperature 2: 50 percent / bromocresol green, NaBH4, HCl / 2 h / -5 °C View Scheme
参考文献
Tarling, Chris A.; Holmes, Andrew B.; Markwell, Roger E.; Pearson, Neil D.
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 12 p. 1695 - 1701
反应条件
1: 66 percent / PPh3, DEAD / tetrahydrofuran / 24 h / Ambient temperature 2: 50 percent / bromocresol green, NaBH4, HCl / 2 h / -5 °C View Scheme
参考文献
Martin, Stephen F.; Liao, Yusheng; Chen, Hui-Ju; Paetzel, Michael; Ramser, Melissa N.
Tetrahedron Letters, 1994 , vol. 35, # 33 p. 6005 - 6008
反应条件
1.1: NaH / dimethylformamide / 1 h / 20 °C 1.2: 83 percent / dimethylformamide / 3 h / 20 °C 2.1: 64 percent / NaBH4; HCl / 2 h / -10 °C View Scheme
参考文献
Tarling, Chris A.; Holmes, Andrew B.; Markwell, Roger E.; Pearson, Neil D.
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 12 p. 1695 - 1701
