3-(4,6,11-三氧杂-1-氮杂-5-硅杂双环[3.3.3]十一烷-5-基)丙-1-胺合成路线 (共 4 条)
参考文献
De, Qing Shi; Chen, Qi; Zhong, Hua Li; Xiao, Peng Liu
Phosphorus, Sulfur and Silicon and the Related Elements, 2005 , vol. 180, # 7 p. 1621 - 1627
反应条件
triethanolamine T=70°C; Dean-Stark;
参考文献
Szpakolski, Katherine; Latham, Kay; Rix, Colin; Rani, Rozina A.; Kalantar-Zadeh, Kourosh
Polyhedron, 2013 , vol. 52, p. 719 - 732
反应条件
bis-trimethylsilyl ether
参考文献
Lukasiak,J. et al.
Roczniki Chemii, 1973 , vol. 47, p. 1975 - 1976
反应条件
1: 1-(3′-aminopropyl)silatrane; dicyclohexyl-carbodiimide in diethyl ether T=0 - 5°C; 0.166667 h; Inert atmosphere; 2: carbon disulfide in diethyl ether T=20°C; Inert atmosphere;
参考文献
Singh, Raghubir; Puri, Jugal Kishore; Chahal, Varinder Kaur; Sharma, Raj Pal; Venugopalan, Paloth
Journal of Organometallic Chemistry, 2010 , vol. 695, # 2 p. 183 - 188