3-(甲氧基甲氧基)-1-丙炔合成路线 （共 10 条）
反应条件
Na-Y-zeolite in dichloromethane 4 h; Heating;
参考文献
Kumari, Pradeep; Raju, Satya V.N.; Reddy, Ravinder S.; Pandey, Bipin
Tetrahedron Letters, 1994 , vol. 35, # 8 p. 1289 - 1290
反应条件
N,N-diethylaniline in dichloromethane from 0 gradC to room temp.;
参考文献
Martin, Stephen F.; Benage, Brigitte; Williamson, Sidney A.; Brown, Stephen P.
Tetrahedron, 1986 , vol. 42, # 11 p. 2903 - 2910
反应条件
toluene-4-sulfonic acid; lithium bromide T=20°C; 24 h;
参考文献
Vrancken, Emmanuel; Alouane, Nacira; Gerard, Helene; Mangeney, Pierre
Journal of Organic Chemistry, 2007 , vol. 72, # 5 p. 1770 - 1779
反应条件
sodium hydride in tetrahydrofuran T=0°C;
参考文献
Tsou; Mamuya; Johnson; Reich; Gruber; Ye; Nilakantan; Shen; Discafani; DeBlanc; Davis; Koehn; Greenberger; Wang; Wissner
Journal of Medicinal Chemistry, 2001 , vol. 44, # 17 p. 2719 - 2734
反应条件
1: propargyl alcohol With sodium hydride in tetrahydrofuran T=0°C; 0.75 h; 2: 1-chloro-2-methoxy-ethane in tetrahydrofuran T=0 - 20°C; Product distribution / selectivity;
参考文献
Wyeth Holdings Corporation
Patent: EP1950201 A1, 2008 ;
Location in patent: Page/Page column 58-59 ;
EP 1950201 A1
参考文献
Shostakovskii,M.F. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1967 , vol. 37, p. 1738 - 1743,1657 - 1661
反应条件
copper(l) iodide; triethylamine; bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran 12 h;
参考文献
Vrancken, Emmanuel; Alouane, Nacira; Gerard, Helene; Mangeney, Pierre
Journal of Organic Chemistry, 2007 , vol. 72, # 5 p. 1770 - 1779
反应条件
n-butyllithium in tetrahydrofuran 20 h; -78 deg C to RT;
参考文献
Journal of the American Chemical Society, , vol. 107, # 13 p. 4072 - 4074
参考文献
Ranu, Brindaban C.; Hajra, Alakananda
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 18 p. 2262 - 2265
反应条件
sodium hydroxide; n-butyllithium; dihydrogen peroxide; boron trichloride in tetrahydrofuran; hexane
1.) -78 deg C to r.t; 2.) -78 deg C to r.t.; 3.) 40 deg C;
参考文献
Carrie; Carrie, Daniel; Carboni; Carboni, Bertrand; Vaultier; Vaultier, Michel
Tetrahedron Letters, 1995 , vol. 36, # 45 p. 8209 - 8212
