3-(4-氯苯基)-2-甲基-4(3H)-喹唑啉酮合成路线 (共 15 条)
反应条件
alum 0.1 h; Microwave irradiationneat (no solvent);
参考文献
Mohammadi, Ali A.; Sadat Hossini
Chinese Journal of Chemistry, 2011 , vol. 29, # 9 p. 1982 - 1984
反应条件
bis(trichloromethyl) carbonate in acetonitrile T=50°C; 15 h;
参考文献
Su; Wu; Xie; Li
Organic Preparations and Procedures International, 2006 , vol. 38, # 1 p. 89 - 94
反应条件
phosphorus pentoxide; N,N-dimethylcyclohexylamine hydrochloride in water T=180°C; 0.583333 h;
参考文献
Hilmy, Khalid Mohamed Hassan; Mogensen, Joergen; Pedersen, Erik B.
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1987 , vol. 41, p. 467 - 468
反应条件
sulfuric acid; silica gel 0.0833333 h; Heatingmicrowave irradiation;
参考文献
Montazeri, Nasser; Rad-Moghadam, Kurosh
Phosphorus, Sulfur and Silicon and the Related Elements, 2004 , vol. 179, # 12 p. 2533 - 2536
反应条件
in tetrahydrofuran T=-78 - 20°C; 3 h;
参考文献
Nakano, Hayato; Kutsumura, Noriki; Saito, Takao
Synthesis (Germany), 2012 , vol. 44, # 20 p. 3179 - 3184
反应条件
in tetrahydrofuran T=-78°C; 1 h;
参考文献
Nakano, Hayato; Kutsumura, Noriki; Saito, Takao
Synthesis (Germany), 2012 , vol. 44, # 20 p. 3179 - 3184
反应条件
in tetrahydrofuran T=-78 - 20°C; 3 h;
参考文献
Nakano, Hayato; Kutsumura, Noriki; Saito, Takao
Synthesis (Germany), 2012 , vol. 44, # 20 p. 3179 - 3184
参考文献
Kumar, Ashok; Sharma, Shalabh; Bajaj, Kiran; Bansal, Deepti; Sharma, Shipra; Saxena, Archana K. K.; Lata; Gupta; Srivastava
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2003 , vol. 42, # 8 p. 1979 - 1984
反应条件
1: dichloromethane / 5 h / 0 - 20 °C 2: tetrahydrofuran / 3 h / -78 - 20 °C View Scheme
参考文献
Nakano, Hayato; Kutsumura, Noriki; Saito, Takao
Synthesis (Germany), 2012 , vol. 44, # 20 p. 3179 - 3184
反应条件
1: dichloromethane / 4 h / 0 - 20 °C / |Inert atmosphere 2: dichloromethane / 5 h / 0 - 20 °C 3: tetrahydrofuran / 3 h / -78 - 20 °C View Scheme
参考文献
Nakano, Hayato; Kutsumura, Noriki; Saito, Takao
Synthesis (Germany), 2012 , vol. 44, # 20 p. 3179 - 3184