(2-氯苯氧基)三甲基硅烷合成路线 (共 12 条)
反应条件
1H-imidazole in N,N-dimethyl-formamide T=25°C; 20 h;
参考文献
Marzi, Elena; Schlosser, Manfred
Tetrahedron, 2005 , vol. 61, # 13 p. 3393 - 3401
反应条件
iodine in chloroform T=60°C; 0.5 h;
参考文献
Hosomi, Akira; Sakurai, Hideki
Chemistry Letters, 1981 , p. 85 - 88
反应条件
18-crown-6 ether; potassium carbonate T=150°C;
参考文献
Renga, James M.; Pen-Chung, Wang
Tetrahedron Letters, 1985 , vol. 26, # 9 p. 1175 - 1178
反应条件
poly(N-bromobenzene-1,3-disulfonamide) 0.05 h; Irradiation;
参考文献
Atkinson, Darcy J.; Sperry, Jonathan; Brimble, Margaret A.
Synthesis, 2010 , # 6 p. 911 - 913
参考文献
Speier
Journal of the American Chemical Society, 1952 , vol. 74, p. 1003,1005
反应条件
sodium 1.) dioxan, reflux, 0.5 h, 2.) dioxan, 20deg C, 15 h; Yield given. Multistep reaction;
参考文献
Heinicke, J.; Nietzschmann, E.; Tzschach, A.
Journal of Organometallic Chemistry, 1983 , vol. 243, # 1 p. 1 - 8
反应条件
pyridine 0.0833333 h;
参考文献
Mulder, Peter; Louw, Robert
Recueil: Journal of the Royal Netherlands Chemical Society, 1984 , vol. 103, # 10 p. 282 - 287
反应条件
heating of (CH3)3SiCl and ClC6H4OH at about 150°C;;
参考文献
Gmelin Handbook: Si: MVol.C, 79, page 219 - 221
Full Text Show Details
Dow Corning Corp.
Patent: US2611778 , 1952 ;
C. A., 1953 , p. 11244
反应条件
1: chloro-trimethyl-silane With sodium in toluene RefluxInert atmosphere; 2: 2-chlorophenol-TMS in toluene RefluxInert atmosphere;
参考文献
Atkinson, Darcy J.; Sperry, Jonathan; Brimble, Margaret A.
Synthesis, 2010 , # 6 p. 911 - 913
反应条件
sodium in toluene in boiling toluene;;
参考文献
Gmelin Handbook: Si: MVol.C, 80, page 222 - 225
Full Text Show Details
Dow Corning Corp.
Patent: US2611799 , 1952 ;
C. A., 1953 , p. 11244