2-(氯甲基)-2,4,4,6,6,8,8-七甲基-环四硅氧烷合成路线 (共 4 条)
反应条件
chlorine in neat (no solvent) Irradiation (UV/VIS); introduction of Cl2 into ((CH3)2SiO)4 under irradiation by light at 25-40°C;;
参考文献
Gmelin Handbook: Si: MVol.C, 99, page 271 - 274
反应条件
tetrachloromethane; meta-chloroperoxybenzoic acid in tetrachloromethane 6 h; Heatingin dry-ice aceton bath;
参考文献
Juengst, Clifford D.; Weber, William P.; Manuel, Georges
Journal of Organometallic Chemistry, 1986 , vol. 308, p. 187 - 194
反应条件
T=25 - 40°C; UV-Licht.Irradiation;
参考文献
Krieble; Elliott
Journal of the American Chemical Society, 1946 , vol. 68, p. 2291
反应条件
iron(III) chloride in neat (no solvent)
heating of C8H23O4ClSi4 with FeCl3*6H2O at 122-140°C;;
参考文献
General Electric Co.
Patent: US2513924 , 1950 ;
C. A., 1950 , p. 9978