2,3-二(三甲基硅基)-1-丙烯合成路线 （共 6 条）
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=60°C; 18 h;
参考文献
Wesquet, Alexander O.; Kazmaier, Uli
Angewandte Chemie - International Edition, 2008 , vol. 47, # 16 p. 3050 - 3053
反应条件
tetrakis(triphenylphosphine) palladium(0) in benzene T=120°C; 20 h;
参考文献
Watanabe, Hamao; Saito, Masayuki; Sutou, Noatake; Kishimito, Kazuya; Inose, Jun; Nagai, Yoichiro
Journal of Organometallic Chemistry, 1982 , vol. 225, # 1 p. 343 - 356
反应条件
magnesium 1.) THF, reflux, 6 h, 2.) THF, reflux 12 h; Yield given. Multistep reaction;
参考文献
Kang; U
Synthetic Communications, 1994 , vol. 24, # 11 p. 1507 - 1512
参考文献
Petrow et al.
Zhurnal Obshchei Khimii, 1956 , vol. 26, p. 1246; engl. Ausg. S. 1409
参考文献
Mironov,V.F. et al.
Doklady Chemistry, 1975 , vol. 222, p. 322 - 325
Dokl. Akad. Nauk SSSR Ser. Khim., 1975 , vol. 222, p. 364 - 367
反应条件
aluminium trichloride 1.) CH2Cl2, -78 deg C, 10 min, 2.) CH2Cl2, -78 deg C, 1 h; Yield given. Multistep reaction;
参考文献
Kang; U
Synthetic Communications, 1994 , vol. 24, # 11 p. 1507 - 1512
