L-亮氨酰-N,3-二甲基-L-缬氨酰胺合成路线 （共 7 条）
反应条件
trifluoroacetic acid in dichloromethane T=20°C; 0.666667 h;
参考文献
Onaran, M. Burak; Comeau, Anthony B.; Seto, Christopher T.
Journal of Organic Chemistry, 2005 , vol. 70, # 26 p. 10792 - 10802
反应条件
1.1: N-hydroxysuccinimide / dimethylformamide / 0.5 h / 20 °C 1.2: 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide hydrochloride / dimethylformamide / 3 h / 0 - 20 °C 2.1: 0.054 g / trifluoroacetic acid / CH2Cl2 / 0.67 h / 20 °C View Scheme
参考文献
France, Stefan; Bernstein, Daniel; Weatherwax, Anthony; Lectka, Thomas
Organic Letters, 2005 , vol. 7, # 14 p. 3009 - 3012
反应条件
tris(2-amimoethyl)amine polystyrene in tetrahydrofuran
参考文献
France, Stefan; Bernstein, Daniel; Weatherwax, Anthony; Lectka, Thomas
Organic Letters, 2005 , vol. 7, # 14 p. 3009 - 3012
反应条件
1: NN'-dicyclohexylcarbodiimide; N'-methylpolystyrene / tetrahydrofuran 2: 0.030 g / tris(2-aminoethyl)amine-polystyrene / tetrahydrofuran View Scheme
参考文献
France, Stefan; Bernstein, Daniel; Weatherwax, Anthony; Lectka, Thomas
Organic Letters, 2005 , vol. 7, # 14 p. 3009 - 3012
反应条件
1.1: N-hydroxysuccinimide / dimethylformamide / 0.5 h / 20 °C 1.2: 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide hydrochloride / dimethylformamide / 3 h / 0 - 20 °C 2.1: 0.054 g / trifluoroacetic acid / CH2Cl2 / 0.67 h / 20 °C View Scheme
参考文献
Onaran, M. Burak; Comeau, Anthony B.; Seto, Christopher T.
Journal of Organic Chemistry, 2005 , vol. 70, # 26 p. 10792 - 10802
反应条件
1.1: N-hydroxysuccinimide / dimethylformamide; methanol / 0.5 h / 20 °C 1.2: 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide hydrochloride / dimethylformamide; methanol / 3 h / 0 - 20 °C 2.1: 0.637 g / trifluoroacetic acid / CH2Cl2 / 0.67 h / 20 °C 3.1: N-hydroxysuccinimide / dimethylformamide / 0.5 h / 20 °C 3.2: 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide hydrochloride / dimethylformamide / 3 h / 0 - 20 °C 4.1: 0.054 g / trifluoroacetic acid / CH2Cl2 / 0.67 h / 20 °C View Scheme
参考文献
Onaran, M. Burak; Comeau, Anthony B.; Seto, Christopher T.
Journal of Organic Chemistry, 2005 , vol. 70, # 26 p. 10792 - 10802
反应条件
1.1: 0.637 g / trifluoroacetic acid / CH2Cl2 / 0.67 h / 20 °C 2.1: N-hydroxysuccinimide / dimethylformamide / 0.5 h / 20 °C 2.2: 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide hydrochloride / dimethylformamide / 3 h / 0 - 20 °C 3.1: 0.054 g / trifluoroacetic acid / CH2Cl2 / 0.67 h / 20 °C View Scheme
参考文献
Onaran, M. Burak; Comeau, Anthony B.; Seto, Christopher T.
Journal of Organic Chemistry, 2005 , vol. 70, # 26 p. 10792 - 10802
