in tetrahydrofuran; diethyl ether T=30°C; Grignard reaction;

[(C5Me5)Sm(CH(SiMe3)2)(C5Me5)K(THF)2]n in toluene T=20°C; 72 h;

yttrium(pentamethylcyclopentadienyl)2CH(trimethylsilyl)2 in benzene 14 h; Ambient temperatureother olefins, other times, other solvents;

bis(cyclopentadienyl)titanium dichloride; n-butyllithium in tetrahydrofuran T=20°C; 1 h;

in diethyl ether T=30°C; 2 h; Inert atmosphere;

1: 1-n-decene With anhydrous iron chloride; tributylphosphine; copper(I) bromide in tetrahydrofuran T=-25°C; 0.0833333 h; Inert atmosphere; 2: 1-ethylbutylmagnesium bromide in tetrahydrofuran; diethyl ether T=-25°C; 0.166667 h; Inert atmosphere; 3: phenyl-chloro-silane in tetrahydrofuran; diethyl ether T=30°C; 2 h; Inert atmosphere;

暂无反应条件数据